dimethyl 2-(2-(2-tosyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)ethyl)malonate

Base Information

Chemical Name:dimethyl 2-(2-(2-tosyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)ethyl)malonate
CAS No.:1478648-84-8
Molecular Formula:C₂₅H₂₈N₂O₆S
Molecular Weight:484.573
Hs Code.:

Synonyms:dimethyl 2-(2-(2-tosyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)ethyl)malonate

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Chemical Property of dimethyl 2-(2-(2-tosyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)ethyl)malonate

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Technology Process of dimethyl 2-(2-(2-tosyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)ethyl)malonate

There total 4 articles about dimethyl 2-(2-(2-tosyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)ethyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1478648-81-5
C₁₈H₂₂N₂O₄

: 98-59-9
p-toluenesulfonyl chloride

: 1478648-84-8
dimethyl 2-(2-(2-tosyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)ethyl)malonate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1055/s-0033-1338969

Reference yield:

: 72473-15-5
formyl-4 methoxycarbonyl-2 butanoate de methyle

: 1478648-84-8
dimethyl 2-(2-(2-tosyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)ethyl)malonate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; water / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With triethylamine; In dichloromethane; water; acetic acid;
DOI:10.1055/s-0036-1592002

Reference yield:

: 61-54-1
tryptamine

: 1478648-84-8
dimethyl 2-(2-(2-tosyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)ethyl)malonate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; water / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With triethylamine; In dichloromethane; water; acetic acid;
DOI:10.1055/s-0036-1592002