(2-(4-((tert-butoxycarbonyl)(methyl)amino)phenyl)benzothiazol-6-yl)(phenyl)iodonium tosylate

Base Information

Chemical Name:(2-(4-((tert-butoxycarbonyl)(methyl)amino)phenyl)benzothiazol-6-yl)(phenyl)iodonium tosylate
CAS No.:1226795-27-2
Molecular Formula:C₇H₇O₃S*C₂₅H₂₄IN₂O₂S
Molecular Weight:714.645
Hs Code.:

Synonyms:(2-(4-((tert-butoxycarbonyl)(methyl)amino)phenyl)benzothiazol-6-yl)(phenyl)iodonium tosylate

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Chemical Property of (2-(4-((tert-butoxycarbonyl)(methyl)amino)phenyl)benzothiazol-6-yl)(phenyl)iodonium tosylate

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Technology Process of (2-(4-((tert-butoxycarbonyl)(methyl)amino)phenyl)benzothiazol-6-yl)(phenyl)iodonium tosylate

There total 1 articles about (2-(4-((tert-butoxycarbonyl)(methyl)amino)phenyl)benzothiazol-6-yl)(phenyl)iodonium tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 1226795-32-9
2-(4'-N-tert-butyloxycarbonyl-methylaminophenyl)-6-tributylstannylbenzothiazole

: 27126-76-7
[hydroxy(tosyloxy)iodo]benzene

: 1226795-27-2
(2-(4-((tert-butoxycarbonyl)(methyl)amino)phenyl)benzothiazol-6-yl)(phenyl)iodonium tosylate

Guidance literature:: In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.03.029

Reference yield:

: 1226795-27-2
(2-(4-((tert-butoxycarbonyl)(methyl)amino)phenyl)benzothiazol-6-yl)(phenyl)iodonium tosylate

: C₁₉H₁₉⁽¹⁸⁾FN₂O₂S

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [18F]-tetrabutylammonium fluoride; In water; acetonitrile; for 0.1h; regioselective reaction; Microwave irradiation;
DOI:10.1016/j.bmc.2011.03.029

Reference yield:

: 1226795-27-2
(2-(4-((tert-butoxycarbonyl)(methyl)amino)phenyl)benzothiazol-6-yl)(phenyl)iodonium tosylate

: 1226795-18-1
2-(4'-N-methylaminophenyl)-6-⁽¹⁸⁾F-fluorobenzothiazole

Guidance literature:: Multi-step reaction with 2 steps

1: [18F]-tetrabutylammonium fluoride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; acetonitrile / 0.1 h / Microwave irradiation

2: hydrogenchloride / water; ethyl acetate / 0.17 h / 75 °C

With hydrogenchloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [18F]-tetrabutylammonium fluoride; In water; ethyl acetate; acetonitrile;
DOI:10.1016/j.bmc.2011.03.029