ethyl 3-(1-hexyl)-4-(4-methoxyphenyl)-2-[N-(4-methoxyphenyl-N-allylamino)]pent-4-enoate

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Chemical Name:ethyl 3-(1-hexyl)-4-(4-methoxyphenyl)-2-[N-(4-methoxyphenyl-N-allylamino)]pent-4-enoate
CAS No.:923293-62-3
Molecular Formula:C₃₀H₄₁NO₄
Molecular Weight:479.66
Hs Code.:

Synonyms:ethyl 3-(1-hexyl)-4-(4-methoxyphenyl)-2-[N-(4-methoxyphenyl-N-allylamino)]pent-4-enoate

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Chemical Property of ethyl 3-(1-hexyl)-4-(4-methoxyphenyl)-2-[N-(4-methoxyphenyl-N-allylamino)]pent-4-enoate

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Technology Process of ethyl 3-(1-hexyl)-4-(4-methoxyphenyl)-2-[N-(4-methoxyphenyl-N-allylamino)]pent-4-enoate

There total 3 articles about ethyl 3-(1-hexyl)-4-(4-methoxyphenyl)-2-[N-(4-methoxyphenyl-N-allylamino)]pent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 923293-52-1
ethyl 3-(1-hexyl)-4-(4-methoxyphenyl)-2-[N-(4-methoxyphenylamino)]pent-4-enoate

: 106-95-6
allyl bromide

: 923293-62-3
ethyl 3-(1-hexyl)-4-(4-methoxyphenyl)-2-[N-(4-methoxyphenyl-N-allylamino)]pent-4-enoate

Guidance literature:: With potassium carbonate; sodium iodide; In acetonitrile; at 80 ℃; for 23h;
DOI:10.1021/ol0624528 DOI:10.1055/s-2007-990845

Reference yield:

: 124156-21-4
ethyl N-(p-methoxyphenyl)iminoacetate

: 923293-62-3
ethyl 3-(1-hexyl)-4-(4-methoxyphenyl)-2-[N-(4-methoxyphenyl-N-allylamino)]pent-4-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / H[P(t-Bu)3]BF₄; CsF / Pd(OAc)2 / tetrahydrofuran / 24 h / 20 °C

2: 78 percent / K₂CO₃; NaI / acetonitrile / 23 h / 80 °C

With potassium carbonate; cesium fluoride; sodium iodide; tri tert-butylphosphoniumtetrafluoroborate; palladium diacetate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ol0624528

Reference yield:

: 104-94-9
4-methoxy-aniline

: 923293-62-3
ethyl 3-(1-hexyl)-4-(4-methoxyphenyl)-2-[N-(4-methoxyphenyl-N-allylamino)]pent-4-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 24 h / 65 °C

2: 54 percent / H[P(t-Bu)3]BF₄; CsF / Pd(OAc)2 / tetrahydrofuran / 24 h / 20 °C

3: 78 percent / K₂CO₃; NaI / acetonitrile / 23 h / 80 °C

With potassium carbonate; cesium fluoride; sodium iodide; tri tert-butylphosphoniumtetrafluoroborate; palladium diacetate; In tetrahydrofuran; acetonitrile; benzene;
DOI:10.1021/ol0624528