(S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-4-benzyloxycarbonyl-butyrylamino]-4-benzyloxycarbonyl-butyrylamino}-4-methyl-pentanoic acid methyl ester; hydrochloride

Base Information

• Chemical Name: (S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-4-benzyloxycarbonyl-butyrylamino]-4-benzyloxycarbonyl-butyrylamino}-4-methyl-pentanoic acid methyl ester; hydrochloride
• CAS No.: 77302-70-6
• Molecular Formula: C₃₇H₅₂N₄O₉*ClH
• Molecular Weight: 733.302

Synonyms:(S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-4-benzyloxycarbonyl-butyrylamino]-4-benzyloxycarbonyl-butyrylamino}-4-methyl-pentanoic acid methyl ester; hydrochloride

Chemical Property of (S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-4-benzyloxycarbonyl-butyrylamino]-4-benzyloxycarbonyl-butyrylamino}-4-methyl-pentanoic acid methyl ester; hydrochloride

Chemical Property:

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Technology Process of (S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-4-benzyloxycarbonyl-butyrylamino]-4-benzyloxycarbonyl-butyrylamino}-4-methyl-pentanoic acid methyl ester; hydrochloride

There total 26 articles about (S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-4-benzyloxycarbonyl-butyrylamino]-4-benzyloxycarbonyl-butyrylamino}-4-methyl-pentanoic acid methyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-2-{(R)-4-Benzyloxycarbonyl-2-[(R)-4-benzyloxycarbonyl-2-((S)-2-tert-butoxycarbonylamino-4-methyl-pentanoylamino)-butyrylamino]-butyrylamino}-4-methyl-pentanoic acid methyl ester (77302-69-3,77302-93-3,77302-94-4) → (S)-2-{(R)-2-[(R)-2-((S)-2-Amino-4-methyl-pentanoylamino)-4-benzyloxycarbonyl-butyrylamino]-4-benzyloxycarbonyl-butyrylamino}-4-methyl-pentanoic acid methyl ester; hydrochloride (77302-70-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 1h; Ambient temperature;

DOI:10.1021/jm00138a013

Reference yield:

(S)-2-{(S)-4-Benzyloxycarbonyl-2-[(R)-4-benzyloxycarbonyl-2-((S)-2-tert-butoxycarbonylamino-4-methyl-pentanoylamino)-butyrylamino]-butyrylamino}-4-methyl-pentanoic acid methyl ester (77302-69-3,77302-93-3,77302-94-4) → (S)-2-{(S)-2-[(R)-2-((S)-2-Amino-4-methyl-pentanoylamino)-4-benzyloxycarbonyl-butyrylamino]-4-benzyloxycarbonyl-butyrylamino}-4-methyl-pentanoic acid methyl ester; hydrochloride (77302-70-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 1h; Ambient temperature;

DOI:10.1021/jm00138a013

Reference yield:

(S)-2-{(R)-4-Benzyloxycarbonyl-2-[(S)-4-benzyloxycarbonyl-2-((S)-2-tert-butoxycarbonylamino-4-methyl-pentanoylamino)-butyrylamino]-butyrylamino}-4-methyl-pentanoic acid methyl ester (77302-69-3,77302-93-3,77302-94-4) → (S)-2-{(R)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-4-benzyloxycarbonyl-butyrylamino]-4-benzyloxycarbonyl-butyrylamino}-4-methyl-pentanoic acid methyl ester; hydrochloride (77302-70-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 1h; Ambient temperature;

DOI:10.1021/jm00138a013

upstream raw materials:

N-(tert-butoxycarbonyl)-L-leucyl-L-γ-O-benzylglutamyl-L-γ-O-benzylglutamyl-L-leucine methyl ester

Boc-Glu(OBzl)-OH

benzyl (S)-4-((tert-butoxycarbonyl)amino)-5-(((S)-1-methoxy-4-methyl-1-oxopentan-2-yl)amino)-5-oxopentanoate

L-γ-O-benzylglutamyl-L-leucine methyl ester hydrochloride

Downstream raw materials:

N-(tert-butoxycarbonyl)-L-phenylalanyl-L-leucyl-L-γ-O-benzylglutamyl-L-γ-O-benzylglutamyl-L-leucine methyl ester

N-(tert-butoxycarbonyl)-L-phenylalanyl-L-leucyl-L-glutamyl-L-glutamyl-L-leucine methyl ester

(S)-2-((S)-4-Benzyloxycarbonyl-2-{(R)-4-benzyloxycarbonyl-2-[(S)-2-((S)-2-tert-butoxycarbonylamino-3-phenyl-propionylamino)-4-methyl-pentanoylamino]-butyrylamino}-butyrylamino)-4-methyl-pentanoic acid methyl ester

Boc-Phe-Leu-D-Glu-Glu-Leu-OMe

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