N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

Base Information

Chemical Name:N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride
CAS No.:1404223-04-6
Molecular Formula:C₁₃H₁₇Cl₂N₅*ClH
Molecular Weight:350.678
Hs Code.:

Synonyms:N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

Chemical Property:

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Technology Process of N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

There total 5 articles about N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1332704-19-4
1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea

: 1404223-04-6
N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

Guidance literature:: With ammonia; mercury dichloride; In methanol; N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jm200503s

Reference yield:

: 19522-67-9
N-isopropylethane-1,2-diamine

: 1404223-04-6
N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 1 h / 0 °C / Inert atmosphere; Reflux

2: triethylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

3: ammonia; mercury dichloride / methanol; N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

With ammonia; triethylamine; mercury dichloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm200503s

Reference yield:

: 766449-90-5
1-isopropyl-4,5-dihydro-1H-imidazol-2-ylamine

: 1404223-04-6
N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

2: ammonia; mercury dichloride / methanol; N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

With ammonia; triethylamine; mercury dichloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm200503s