1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea

Base Information

Chemical Name:1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea
CAS No.:1332704-19-4
Molecular Formula:C₁₃H₁₆Cl₂N₄S
Molecular Weight:331.269
Hs Code.:

Synonyms:1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea

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Technology Process of 1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea

There total 3 articles about 1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 766449-90-5
1-isopropyl-4,5-dihydro-1H-imidazol-2-ylamine

: 6590-94-9
3,4-dichlorophenyl isothiocyanate

: 1332704-20-7
2-imino-3-isopropyl-imidazolidine-1-carbothioic acid (3,4-dichlorophenyl)amide

: 1332704-19-4
1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 72h; Inert atmosphere;
DOI:10.1021/jm200503s

Reference yield:

: 19522-67-9
N-isopropylethane-1,2-diamine

: 1332704-20-7
2-imino-3-isopropyl-imidazolidine-1-carbothioic acid (3,4-dichlorophenyl)amide

: 1332704-19-4
1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 1 h / 0 °C / Inert atmosphere; Reflux

2: triethylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

With triethylamine; In methanol; dichloromethane;
DOI:10.1021/jm200503s

Reference yield:

: 61682-19-7
1-isopropyl-2-methylmercapto-imidazoline

: 1332704-20-7
2-imino-3-isopropyl-imidazolidine-1-carbothioic acid (3,4-dichlorophenyl)amide

: 1332704-19-4
1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / Inert atmosphere; Reflux

2: triethylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

With ammonium hydroxide; triethylamine; In dichloromethane;
DOI:10.1021/jm200503s