(3αR,5S,6αR)-5-(benzyloxymethyl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

Base Information

Chemical Name:(3αR,5S,6αR)-5-(benzyloxymethyl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole
CAS No.:116306-89-9
Molecular Formula:C₁₅H₂₀O₄
Molecular Weight:264.321
Hs Code.:

Synonyms:(3αR,5S,6αR)-5-(benzyloxymethyl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

Suppliers and Price of (3αR,5S,6αR)-5-(benzyloxymethyl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3αR,5S,6αR)-5-(benzyloxymethyl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

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Technology Process of (3αR,5S,6αR)-5-(benzyloxymethyl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

There total 14 articles about (3αR,5S,6αR)-5-(benzyloxymethyl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 3396-71-2
3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

: 100-44-7
benzyl chloride

: 116306-89-9
(3αR,5S,6αR)-5-(benzyloxymethyl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

Guidance literature:: 3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1h;

benzyl chloride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2010.11.038

Reference yield: 95.0%

: 3396-71-2
3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

: 100-39-0
benzyl bromide

: 116306-89-9
(3αR,5S,6αR)-5-(benzyloxymethyl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield: 69.0%

: 14260-66-3
((3αR,5S,6αR)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanol

: 100-39-0
benzyl bromide

: 116306-89-9
(3αR,5S,6αR)-5-(benzyloxymethyl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

Guidance literature:: ((3αR,5S,6αR)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.416667h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; for 2h;