N'-(4-chlorophenylsulfonyl)-N-(4-hydroxy-2,5-dimethylphenyl)benzimidamide

Base Information

Chemical Name:N'-(4-chlorophenylsulfonyl)-N-(4-hydroxy-2,5-dimethylphenyl)benzimidamide
CAS No.:1332847-25-2
Molecular Formula:C₂₁H₁₉ClN₂O₃S
Molecular Weight:414.912
Hs Code.:

Synonyms:N'-(4-chlorophenylsulfonyl)-N-(4-hydroxy-2,5-dimethylphenyl)benzimidamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(4-chlorophenylsulfonyl)-N-(4-hydroxy-2,5-dimethylphenyl)benzimidamide

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Technology Process of N'-(4-chlorophenylsulfonyl)-N-(4-hydroxy-2,5-dimethylphenyl)benzimidamide

There total 1 articles about N'-(4-chlorophenylsulfonyl)-N-(4-hydroxy-2,5-dimethylphenyl)benzimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 3096-71-7
2,5-dimethyl-4-amino phenol

: 4513-26-2
N-p-chlorophenylsulfonylbenzimidoyl chloride

: 1332847-25-2
N'-(4-chlorophenylsulfonyl)-N-(4-hydroxy-2,5-dimethylphenyl)benzimidamide

Guidance literature:: With sodium acetate; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1134/S107042801207007X

Reference yield: 89.0%

: 1332847-25-2
N'-(4-chlorophenylsulfonyl)-N-(4-hydroxy-2,5-dimethylphenyl)benzimidamide

: 1332847-20-7
N'-(4-chlorophenylsulfonyl)-N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)benzenecarboximidamide

Guidance literature:: With lead(IV) tetraacetate; In acetic acid;
DOI:10.1134/S1070428011070116

Reference yield:

: 1332847-25-2
N'-(4-chlorophenylsulfonyl)-N-(4-hydroxy-2,5-dimethylphenyl)benzimidamide

: 1332847-77-4
N-(3-bromo-2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-chlorophenylsulfonyl)benzenecarboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1: lead(IV) tetraacetate / acetic acid

2: hydrogen bromide / water; acetic acid / 50 - 60 °C

3: lead(IV) tetraacetate / acetic acid / 20 °C

With hydrogen bromide; lead(IV) tetraacetate; In water; acetic acid;
DOI:10.1134/S1070428011070116