N-(3-bromo-4-hydroxy-2,5-dimethylphenyl)-N'-(4-chlorophenylsulfonyl)benzenecarboximidamide

Base Information

Chemical Name:N-(3-bromo-4-hydroxy-2,5-dimethylphenyl)-N'-(4-chlorophenylsulfonyl)benzenecarboximidamide
CAS No.:1332847-64-9
Molecular Formula:C₂₁H₁₈BrClN₂O₃S
Molecular Weight:493.809
Hs Code.:

Synonyms:N-(3-bromo-4-hydroxy-2,5-dimethylphenyl)-N'-(4-chlorophenylsulfonyl)benzenecarboximidamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-bromo-4-hydroxy-2,5-dimethylphenyl)-N'-(4-chlorophenylsulfonyl)benzenecarboximidamide

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Technology Process of N-(3-bromo-4-hydroxy-2,5-dimethylphenyl)-N'-(4-chlorophenylsulfonyl)benzenecarboximidamide

There total 4 articles about N-(3-bromo-4-hydroxy-2,5-dimethylphenyl)-N'-(4-chlorophenylsulfonyl)benzenecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1332847-20-7
N'-(4-chlorophenylsulfonyl)-N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)benzenecarboximidamide

: 1332847-64-9
N-(3-bromo-4-hydroxy-2,5-dimethylphenyl)-N'-(4-chlorophenylsulfonyl)benzenecarboximidamide

Guidance literature:: With hydrogen bromide; In water; acetic acid; at 50 - 60 ℃;
DOI:10.1134/S1070428011070116

Reference yield:

: 1332847-25-2
N'-(4-chlorophenylsulfonyl)-N-(4-hydroxy-2,5-dimethylphenyl)benzimidamide

: 1332847-64-9
N-(3-bromo-4-hydroxy-2,5-dimethylphenyl)-N'-(4-chlorophenylsulfonyl)benzenecarboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: lead(IV) tetraacetate / acetic acid

2: hydrogen bromide / water; acetic acid / 50 - 60 °C

With hydrogen bromide; lead(IV) tetraacetate; In water; acetic acid;
DOI:10.1134/S1070428011070116

Reference yield:

: 4513-26-2
N-p-chlorophenylsulfonylbenzimidoyl chloride

: 1332847-64-9
N-(3-bromo-4-hydroxy-2,5-dimethylphenyl)-N'-(4-chlorophenylsulfonyl)benzenecarboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / acetic acid; N,N-dimethyl-formamide

2: bromine / chloroform / 24 h / 40 - 50 °C

With bromine; sodium acetate; In chloroform; acetic acid; N,N-dimethyl-formamide;
DOI:10.1134/S107042801207007X