C₂H₂NIrO(O)(C₅(CH₃)5)(SO₂C₆H₄CH₃)

Base Information

• Chemical Name: C₂H₂NIrO(O)(C₅(CH₃)5)(SO₂C₆H₄CH₃)
• CAS No.: 157699-57-5
• Molecular Formula: C₁₉H₂₄IrNO₄S
• Molecular Weight: 554.69

Synonyms:C₂H₂NIrO(O)(C₅(CH₃)5)(SO₂C₆H₄CH₃)

Chemical Property of C₂H₂NIrO(O)(C₅(CH₃)5)(SO₂C₆H₄CH₃)

Chemical Property:

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Technology Process of C₂H₂NIrO(O)(C₅(CH₃)5)(SO₂C₆H₄CH₃)

There total 2 articles about C₂H₂NIrO(O)(C₅(CH₃)5)(SO₂C₆H₄CH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

bis((μ-chloro)chloro(pentamethylcyclopentadienyl)iridium) + N-Tosylglycine (1080-44-0) → C2H2NIrO(O)(C5(CH3)5)(SO2C6H4CH3) (157699-57-5)

Guidance literature:

With K₂CO₃; In acetonitrile; N2-atmosphere, 5 h; concg., extg. (CH2Cl2), filtering, washing (CH2Cl2), concg., drying (vac.); elem. anal.;

DOI:10.1021/om00008a014

Reference yield:

bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] (12354-84-6,12354-85-7) + N-Tosylglycine (1080-44-0) → C2H2NIrO(O)(C5(CH3)5)(SO2C6H4CH3) (157699-57-5)

Guidance literature:

With K₂CO₃; In not given; under N2, in THF or CH3CN, stirred for 4-36 h; filtd., the filtrate is concd.;

DOI:10.1021/ja00094a075

Reference yield: 100.0%

C2H2NIrO(O)(C5(CH3)5)(SO2C6H4CH3) (157699-57-5) + carbon monoxide (201230-82-2) → [(η5-C5Me5)Ir(CO)(η2-(N,O)-TsNCH2CO2)]

Guidance literature:

In chloroform-d1; NMR tube, CO-bubbling (2 min);

DOI:10.1021/om00008a014

upstream raw materials:

N-Tosylglycine

bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]

Downstream raw materials:

((CH₃)5C₅)Ir(P(C₆H₅)3)(C₂H₂O₂NSO₂C₆H₄CH₃)

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