Methyl-[5-(2-trifluoromethyl-phenyl)-[1,3,4]thiadiazol-2-yl]-dithiocarbamic acid methyl ester

Base Information

Chemical Name:Methyl-[5-(2-trifluoromethyl-phenyl)-[1,3,4]thiadiazol-2-yl]-dithiocarbamic acid methyl ester
CAS No.:107114-97-6
Molecular Formula:C₁₂H₁₀F₃N₃S₃
Molecular Weight:349.425
Hs Code.:

Synonyms:Methyl-[5-(2-trifluoromethyl-phenyl)-[1,3,4]thiadiazol-2-yl]-dithiocarbamic acid methyl ester

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Chemical Property of Methyl-[5-(2-trifluoromethyl-phenyl)-[1,3,4]thiadiazol-2-yl]-dithiocarbamic acid methyl ester

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Technology Process of Methyl-[5-(2-trifluoromethyl-phenyl)-[1,3,4]thiadiazol-2-yl]-dithiocarbamic acid methyl ester

There total 5 articles about Methyl-[5-(2-trifluoromethyl-phenyl)-[1,3,4]thiadiazol-2-yl]-dithiocarbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107115-00-4
2-chloro-5-[2-(trifluoromethyl)phenyl]-1,3,4-thiadiazole

: 107114-97-6
Methyl-[5-(2-trifluoromethyl-phenyl)-[1,3,4]thiadiazol-2-yl]-dithiocarbamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / H₂O; dioxane / 18 h / Ambient temperature

2: sodium methoxide / 120 h / Ambient temperature

3: H₂O; dimethylformamide / 3 h

With sodium methylate; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00388a038

Reference yield:

: 107114-93-2
2-(methylamino)-5-<2-(trifluoromethyl)phenyl>-1,3,4-thiadiazole

: 107114-97-6
Methyl-[5-(2-trifluoromethyl-phenyl)-[1,3,4]thiadiazol-2-yl]-dithiocarbamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methoxide / 120 h / Ambient temperature

2: H₂O; dimethylformamide / 3 h

With sodium methylate; In water; N,N-dimethyl-formamide;
DOI:10.1021/jm00388a038

Reference yield:

: 107114-95-4
2-(methylcyanamido)-5-<2-(trifluoromethyl)phenyl>-1,3,4-thiadiazole

: 107114-97-6
Methyl-[5-(2-trifluoromethyl-phenyl)-[1,3,4]thiadiazol-2-yl]-dithiocarbamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: ammonia / 16 h / 110 °C

2: sodium methoxide / 120 h / Ambient temperature

3: H₂O; dimethylformamide / 3 h

With ammonia; sodium methylate; In water; N,N-dimethyl-formamide;
DOI:10.1021/jm00388a038