methyl 2-(acetylamino)-6-deoxy-5,6-didehydro-3-O-<(2-methoxyethoxy)methyl>-α-D-galactopyranoside

Base Information

Chemical Name:methyl 2-(acetylamino)-6-deoxy-5,6-didehydro-3-O-<(2-methoxyethoxy)methyl>-α-D-galactopyranoside
CAS No.:137233-52-4
Molecular Formula:C₁₃H₂₃NO₇
Molecular Weight:305.328
Hs Code.:

Synonyms:methyl 2-(acetylamino)-6-deoxy-5,6-didehydro-3-O-<(2-methoxyethoxy)methyl>-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-(acetylamino)-6-deoxy-5,6-didehydro-3-O-<(2-methoxyethoxy)methyl>-α-D-galactopyranoside

Chemical Property:

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Technology Process of methyl 2-(acetylamino)-6-deoxy-5,6-didehydro-3-O-<(2-methoxyethoxy)methyl>-α-D-galactopyranoside

There total 1 articles about methyl 2-(acetylamino)-6-deoxy-5,6-didehydro-3-O-<(2-methoxyethoxy)methyl>-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137233-51-3,137331-08-9
C₅₀H₇₉N₃O₁₄SeSi₃

: 137233-52-4
methyl 2-(acetylamino)-6-deoxy-5,6-didehydro-3-O-<(2-methoxyethoxy)methyl>-α-D-galactopyranoside

: 137233-58-0,137330-29-1
C₄₂H₇₁N₃O₁₄Si₂

: 137233-58-0
C₄₂H₇₁N₃O₁₄Si₂

Guidance literature:: With potassium fluoride; triethyl borane; tri-n-butyl-tin hydride; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₃CN, from -10 to 23 deg C, 2.) methanol;
DOI:10.1021/ja00025a036

Reference yield:

: 137233-52-4
methyl 2-(acetylamino)-6-deoxy-5,6-didehydro-3-O-<(2-methoxyethoxy)methyl>-α-D-galactopyranoside

: 1-{(2R,3R,4R,5S)-3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-5-[(chloro-dimethyl-silanyloxy)-phenylselanyl-methyl]-tetrahydro-furan-2-yl}-3-(4-methoxy-benzyl)-1H-pyrimidine-2,4-dione

: 137233-51-3,137331-08-9
C₅₀H₇₉N₃O₁₄SeSi₃

Guidance literature:: With pyridine; In toluene; at 23 ℃; for 0.166667h; Yield given;
DOI:10.1021/ja00090a018

Reference yield:

: 137233-52-4
methyl 2-(acetylamino)-6-deoxy-5,6-didehydro-3-O-<(2-methoxyethoxy)methyl>-α-D-galactopyranoside

: 137233-58-0
C₄₂H₇₁N₃O₁₄Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / toluene / 0.17 h / 23 °C

2: 1.) triethylborane, tributyltin hydride, 2.) potassium fluoride hydrate / 1.) hexane, acetonitrile, -8 deg C, 30 min, 2.) MeOH, 23 deg C, 5 h

With pyridine; potassium fluoride; triethyl borane; tri-n-butyl-tin hydride; In toluene;
DOI:10.1021/ja00090a018