methyl 3-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]propionate

Base Information

Chemical Name:methyl 3-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]propionate
CAS No.:558472-39-2
Molecular Formula:C₂₇H₂₈Cl₂O₄S
Molecular Weight:521.478
Hs Code.:

Synonyms:methyl 3-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]propionate

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Chemical Property of methyl 3-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]propionate

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Technology Process of methyl 3-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]propionate

There total 1 articles about methyl 3-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 5597-50-2
3-(4-hydroxyphenyl)propionic acid methyl ester

: 2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethanol

: 558472-39-2
methyl 3-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]propionate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; at 20 ℃; for 18h;
DOI:10.1002/jlcr.655

Reference yield: 86.0%

: 558472-39-2
methyl 3-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]propionate

: 3-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]propionic acid

Guidance literature:: With potassium hydroxide; In ethanol; water; at 60 ℃; for 1h;
DOI:10.1002/jlcr.655

Reference yield:

: 407-25-0
trifluoroacetic anhydride

: 558472-39-2
methyl 3-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]propionate

: 4-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]-1,1,1-trifluoro-2-butanone

Guidance literature:: methyl 3-[4-[2-[2-[bis(4-chlorophenyl)methoxy]ethylthio][1-14C]ethoxy]phenyl]propionate; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 1h;

trifluoroacetic anhydride; With pyridine; In toluene; at 20 ℃; for 2h;
DOI:10.1002/jlcr.655