2-(2-{3-[2-(2-Hydroxy-ethoxy)-phenoxy]-naphthalen-2-yloxy}-phenoxy)-ethanol

Base Information

Chemical Name:2-(2-{3-[2-(2-Hydroxy-ethoxy)-phenoxy]-naphthalen-2-yloxy}-phenoxy)-ethanol
CAS No.:131354-83-1
Molecular Formula:C₂₆H₂₄O₆
Molecular Weight:432.473
Hs Code.:

Synonyms:2-(2-{3-[2-(2-Hydroxy-ethoxy)-phenoxy]-naphthalen-2-yloxy}-phenoxy)-ethanol

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Chemical Property of 2-(2-{3-[2-(2-Hydroxy-ethoxy)-phenoxy]-naphthalen-2-yloxy}-phenoxy)-ethanol

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Technology Process of 2-(2-{3-[2-(2-Hydroxy-ethoxy)-phenoxy]-naphthalen-2-yloxy}-phenoxy)-ethanol

There total 5 articles about 2-(2-{3-[2-(2-Hydroxy-ethoxy)-phenoxy]-naphthalen-2-yloxy}-phenoxy)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 131354-78-4
2,3-Bis-[2-(2-benzyloxy-ethoxy)-phenoxy]-naphthalene

: 131354-83-1
2-(2-{3-[2-(2-Hydroxy-ethoxy)-phenoxy]-naphthalen-2-yloxy}-phenoxy)-ethanol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 25 ℃; for 4h; under 2280 Torr;
DOI:10.1021/jo00003a055

Reference yield:

: 13214-70-5
2,3-dibromonaphthalene

: 131354-83-1
2-(2-{3-[2-(2-Hydroxy-ethoxy)-phenoxy]-naphthalen-2-yloxy}-phenoxy)-ethanol

Guidance literature:: Multi-step reaction with 4 steps

1: 35.8 percent / CuO₂, 1,3-dimethylimidazolin-2-one / 46 h / 170 - 180 °C

2: 97 percent / BBr₃ / CH₂Cl₂ / 3 h / 0 °C

3: 1.) Cs₂CO₃ / 1.) DMF, 80 deg C, 1 h, 2.) 80 deg C, 6 h

4: 82 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 4 h / 25 °C / 2280 Torr

With 1,3-dimethyl-2-imidazolinone; hydrogen; boron tribromide; caesium carbonate; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jo00003a055

Reference yield:

: 131354-69-3
C₂₂H₁₆O₄

: 131354-83-1
2-(2-{3-[2-(2-Hydroxy-ethoxy)-phenoxy]-naphthalen-2-yloxy}-phenoxy)-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Cs₂CO₃ / 1.) DMF, 80 deg C, 1 h, 2.) 80 deg C, 6 h

2: 82 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 4 h / 25 °C / 2280 Torr

With hydrogen; caesium carbonate; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/jo00003a055