Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid

Base Information

• Chemical Name: Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid
• CAS No.: 75788-40-8
• Molecular Formula: C₂₂H₂₃NO₅
• Molecular Weight: 381.428

Synonyms:Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid

Chemical Property of Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid

Chemical Property:

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SDS file from LookChem

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Technology Process of Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid

There total 3 articles about Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

benzyl 2-acetamido 4,6-O-benzylidene-2-deoxy-3-O-mesyl-α-D-allopyranoside (75788-39-5) → Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-α-D-glucopyranoside (13343-65-2) + Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid (75788-40-8) + Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-3-enopyranosid (75788-41-9)

Guidance literature:

With DBN; In N,N-dimethyl-formamide; at 80 ℃; for 7h;

Reference yield: 70.0%

benzyl 2-acetamido 4,6-O-benzylidene-2-deoxy-3-O-mesyl-α-D-allopyranoside (75788-39-5) → Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid (75788-40-8)

Guidance literature:

With tetrabutyl ammonium fluoride; In acetonitrile; for 4h; Heating;

DOI:10.1016/0008-6215(93)84174-5

Reference yield: 36.0%

benzyl 2-acetamido 4,6-O-benzylidene-2-deoxy-3-O-mesyl-α-D-allopyranoside (75788-39-5) → Benzyl-2-acetylamino-3-azido-4,6-O-benzyliden-2,3-didesoxy-α-D-glucopyranosid (27539-63-5) + Benzyl-2-acetylamino-4,6-O-benzyliden-2-desoxy-α-D-allopyranosid (27539-62-4) + Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid (75788-40-8) + Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-3-enopyranosid (75788-41-9)

Guidance literature:

With sodium azide; In water; N,N-dimethyl-formamide; for 0.0166667h; Heating;

upstream raw materials:

benzyl 2-acetamido 4,6-O-benzylidene-2-deoxy-3-O-mesyl-α-D-allopyranoside

Downstream raw materials:

benzyl 4,6-O-benzylidene-2-acetylamino-2-deoxy-α-D-glucopyranoside

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