Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-α-D-glucopyranoside

Base Information

• Chemical Name: Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-α-D-glucopyranoside
• CAS No.: 13343-65-2
• Molecular Formula: C₂₃H₂₇NO₈S
• Molecular Weight: 477.535

Synonyms:Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-α-D-glucopyranoside

Chemical Property of Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-α-D-glucopyranoside

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Technology Process of Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-α-D-glucopyranoside

There total 1 articles about Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

benzyl 2-acetamido 4,6-O-benzylidene-2-deoxy-3-O-mesyl-α-D-allopyranoside (75788-39-5) → Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-α-D-glucopyranoside (13343-65-2) + Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid (75788-40-8) + Benzyl-2-acetylamino-4,6-O-benzyliden-2,3-didesoxy-α-D-erythro-hex-3-enopyranosid (75788-41-9)

Guidance literature:

With DBN; In N,N-dimethyl-formamide; at 80 ℃; for 7h;

Reference yield: 75.0%

Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-α-D-glucopyranoside (13343-65-2) → benzyl 2-acetamido-2-deoxy-3-O-methylsulfonyl-α-D-glucopyranoside (74024-08-1)

Guidance literature:

With water; In acetic acid; at 90 ℃; for 1h;

DOI:10.1016/S0008-6215(00)85130-7

Reference yield: 68.0%

Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-α-D-glucopyranoside (13343-65-2) → 1'-O-Benzyl-4',6'-O-benzyliden-2'-desoxy-2-methyl-α-D-allopyranosido<2',3':4,5>-2-oxazolin (73793-22-3)

Guidance literature:

With potassium cyanide; In N,N-dimethyl-formamide; for 15h; Heating;

upstream raw materials:

benzyl 2-acetamido 4,6-O-benzylidene-2-deoxy-3-O-mesyl-α-D-allopyranoside

Downstream raw materials:

1'-O-Benzyl-4',6'-O-benzyliden-2'-desoxy-2-methyl-α-D-allopyranosido<2',3':4,5>-2-oxazolin

benzyl 4,6-O-benzylidene-2,3-dideoxy-2,3-epimino-α-D-allopyranoside

benzyl 2-acetamido-2-deoxy-3-O-methylsulfonyl-α-D-glucopyranoside

Benzyl-4,6-di-O-acetyl-2-acetylamino-2-desoxy-3-O-methylsulfonyl-α-D-glucopyranosid

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