C₃₁H₄₃N₃O₅SSi

Base Information

Chemical Name:C₃₁H₄₃N₃O₅SSi
CAS No.:1174231-52-7
Molecular Formula:C₃₁H₄₃N₃O₅SSi
Molecular Weight:597.851
Hs Code.:

C<sub>31</sub>H<sub>43</sub>N<sub>3</sub>O<sub>5</sub>SSi

Synonyms:C₃₁H₄₃N₃O₅SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₄₃N₃O₅SSi

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Technology Process of C₃₁H₄₃N₃O₅SSi

There total 10 articles about C₃₁H₄₃N₃O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 886860-04-4
5-({[tert-butyl(dimethyl)silyl]oxy}methyl)pyrazin-2-amine

: C₂₀H₂₃ClO₄S

: 1174231-52-7
C₃₁H₄₃N₃O₅SSi

Guidance literature:: With pyridine; In dichloromethane; for 0.333333h; Cooling with ice;

Reference yield:

: 33332-25-1
methyl 5-chloropyrazine-2-carboxylate

: 1174231-52-7
C₃₁H₄₃N₃O₅SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / water / 20 °C / Inert atmosphere

2.1: oxalyl dichloride / N,N-dimethyl-formamide; 1,4-dioxane / 20 °C / Inert atmosphere

2.2: 5 °C / Inert atmosphere

3.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 12 °C / Inert atmosphere; Industrial scale

4.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 70 °C / Inert atmosphere

5.1: Wilkinson's catalyst / acetonitrile; water / 100 °C / Inert atmosphere

6.1: N,N-dimethyl-formamide; dichloromethane / 3 h / -3 - -1 °C / Inert atmosphere; Industrial scale

With 1H-imidazole; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; Wilkinson's catalyst; oxalyl dichloride; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium hydroxide; sodium t-butanolate; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/acs.oprd.6b00415

Reference yield:

: 1174229-45-8
methyl 2-[3-bromo-4-(cyclopropylsulfonyl)phenyl]-3-[(2R,3R,7R)-2,3-diphenyl-1,4-dioxaspiro[4.4]non-7-yl]propionate

: 1174231-52-7
C₃₁H₄₃N₃O₅SSi

Guidance literature:: Multi-step reaction with 5 steps

1: palladium diacetate; triphenylphosphine; potassium phosphate / toluene; water / 20 h / 87 °C / Inert atmosphere; Industrial scale

2: sodium hydroxide / methanol; tetrahydrofuran; water / 2 h / 47 °C / Inert atmosphere; Industrial scale

3: hydrogenchloride / water; acetone / 50 °C / Inert atmosphere; Industrial scale

4: dmap; pyridine; trichlorophosphate / N,N-dimethyl-formamide; dichloromethane / 1 h / -4 - -3 °C / Inert atmosphere; Industrial scale

5: N,N-dimethyl-formamide; dichloromethane / 3 h / -3 - -1 °C / Inert atmosphere; Industrial scale

With pyridine; hydrogenchloride; dmap; potassium phosphate; palladium diacetate; triphenylphosphine; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; 1: |Suzuki Coupling;
DOI:10.1021/acs.oprd.6b00415