1,4-bis(3-((3aR,5R,6S,6aR)-6-(Benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propyl)benzene

Base Information

Chemical Name:1,4-bis(3-((3aR,5R,6S,6aR)-6-(Benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propyl)benzene
CAS No.:1355953-49-9
Molecular Formula:C₄₀H₅₀O₈
Molecular Weight:658.832
Hs Code.:

Synonyms:1,4-bis(3-((3aR,5R,6S,6aR)-6-(Benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propyl)benzene

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Chemical Property of 1,4-bis(3-((3aR,5R,6S,6aR)-6-(Benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propyl)benzene

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Technology Process of 1,4-bis(3-((3aR,5R,6S,6aR)-6-(Benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propyl)benzene

There total 5 articles about 1,4-bis(3-((3aR,5R,6S,6aR)-6-(Benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₀H₄₆O₈

: 1355953-49-9
1,4-bis(3-((3aR,5R,6S,6aR)-6-(Benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propyl)benzene

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 24h;
DOI:10.1016/j.carres.2011.11.005

Reference yield:

: 1355953-27-3
2-((2-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethyl)sulfonyl)benzo[d]thiazole

: 1355953-49-9
1,4-bis(3-((3aR,5R,6S,6aR)-6-(Benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 24 h / 20 °C

With palladium 10% on activated carbon; hydrogen; sodium hydride; In ethyl acetate; N,N-dimethyl-formamide; 1: Julia Olefin synthesis;
DOI:10.1016/j.carres.2011.11.005

Reference yield:

: 1355953-25-1
C₁₆H₂₁BrO₄

: 1355953-49-9
1,4-bis(3-((3aR,5R,6S,6aR)-6-(Benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / tetrahydrofuran / 0 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C / Molecular sieve; Inert atmosphere

3: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

4: palladium 10% on activated carbon; hydrogen / ethyl acetate / 24 h / 20 °C

With palladium 10% on activated carbon; hydrogen; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 3: Julia Olefin synthesis;
DOI:10.1016/j.carres.2011.11.005