3,9-difluoro-6-(4-tert-butylbenzyl)-12,13-dihydro-12-(2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)indolo[2,3-a]-pyrrolo[3,4-c]carbazole-5,7-dione

Base Information

Chemical Name:3,9-difluoro-6-(4-tert-butylbenzyl)-12,13-dihydro-12-(2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)indolo[2,3-a]-pyrrolo[3,4-c]carbazole-5,7-dione
CAS No.:849824-62-0
Molecular Formula:C₅₈H₄₅F₂N₃O₁₀
Molecular Weight:982.006
Hs Code.:

Synonyms:3,9-difluoro-6-(4-tert-butylbenzyl)-12,13-dihydro-12-(2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)indolo[2,3-a]-pyrrolo[3,4-c]carbazole-5,7-dione

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Chemical Property of 3,9-difluoro-6-(4-tert-butylbenzyl)-12,13-dihydro-12-(2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)indolo[2,3-a]-pyrrolo[3,4-c]carbazole-5,7-dione

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Technology Process of 3,9-difluoro-6-(4-tert-butylbenzyl)-12,13-dihydro-12-(2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)indolo[2,3-a]-pyrrolo[3,4-c]carbazole-5,7-dione

There total 4 articles about 3,9-difluoro-6-(4-tert-butylbenzyl)-12,13-dihydro-12-(2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)indolo[2,3-a]-pyrrolo[3,4-c]carbazole-5,7-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₅H₅₇F₂N₃O₇

: 849824-62-0
3,9-difluoro-6-(4-tert-butylbenzyl)-12,13-dihydro-12-(2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)indolo[2,3-a]-pyrrolo[3,4-c]carbazole-5,7-dione

Guidance literature:: Multi-step reaction with 2 steps

1: cyclohexene / Pd(OH)2/C / ethanol / Heating

2: pyridine / 0.33 h / -5 °C

With pyridine; cyclohexene; palladium dihydroxide; In ethanol;
DOI:10.1021/jm049090z

Reference yield:

: 6386-24-9
2,3,4,6-tetra-O-benzyl-D-galactopyranose

: 849824-62-0
3,9-difluoro-6-(4-tert-butylbenzyl)-12,13-dihydro-12-(2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)indolo[2,3-a]-pyrrolo[3,4-c]carbazole-5,7-dione

Guidance literature:: Multi-step reaction with 3 steps

1: Ph₃P; DIAD / tetrahydrofuran

2: cyclohexene / Pd(OH)2/C / ethanol / Heating

3: pyridine / 0.33 h / -5 °C

With pyridine; di-isopropyl azodicarboxylate; triphenylphosphine; cyclohexene; palladium dihydroxide; In tetrahydrofuran; ethanol; 1: Mitsunobu reaction;
DOI:10.1021/jm049090z

Reference yield:

: 204194-33-2
C₃₁H₂₃F₂N₃O₂

: 849824-62-0
3,9-difluoro-6-(4-tert-butylbenzyl)-12,13-dihydro-12-(2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)indolo[2,3-a]-pyrrolo[3,4-c]carbazole-5,7-dione

Guidance literature:: Multi-step reaction with 3 steps

1: Ph₃P; DIAD / tetrahydrofuran

2: cyclohexene / Pd(OH)2/C / ethanol / Heating

3: pyridine / 0.33 h / -5 °C

With pyridine; di-isopropyl azodicarboxylate; triphenylphosphine; cyclohexene; palladium dihydroxide; In tetrahydrofuran; ethanol; 1: Mitsunobu reaction;
DOI:10.1021/jm049090z