2-(2,4-dichlorophenoxy)-N-propylacetamide

Base Information

• Chemical Name: 2-(2,4-dichlorophenoxy)-N-propylacetamide
• CAS No.: 73413-66-8
• Molecular Formula: C₁₁H₁₃Cl₂NO₂
• Molecular Weight: 262.136
• DSSTox Substance ID: DTXSID501339116

Synonyms:2-(2,4-dichlorophenoxy)-N-propylacetamide;Oprea1_213744;DTXSID501339116;AKOS003848849;73413-66-8

Chemical Property of 2-(2,4-dichlorophenoxy)-N-propylacetamide

Chemical Property:

• XLogP3: 3.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 261.0323340
• Heavy Atom Count: 16
• Complexity: 226

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCCNC(=O)COC1=C(C=C(C=C1)Cl)Cl

Technology Process of 2-(2,4-dichlorophenoxy)-N-propylacetamide

There total 2 articles about 2-(2,4-dichlorophenoxy)-N-propylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(propyl)chloroacetamide (13916-39-7) + 2,4-dichlorophenol (120-83-2,40477-79-0) → 2-(2,4-dichlorophenoxy)-N-propyl-acetamide (73413-66-8)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; Reflux;

DOI:10.1002/bkcs.11673

Reference yield:

→ 2-(2,4-dichlorophenoxy)-N-propyl-acetamide (73413-66-8)

Guidance literature:

Hydroxamsaeure Ib (Y=Cl), Propylhalogenid;

Reference yield:

2-(2,4-dichlorophenoxy)-N-propyl-acetamide (73413-66-8) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → (E)-N-propyl-N-(1-chloro-2-(2,4-dichlorophenoxy)vinyl)formamide + (Z)-N-propyl-N-(1-chloro-2-(2,4-dichlorophenoxy)vinyl)formamide

Guidance literature:

With trichlorophosphate; at 0 - 40 ℃; for 6h; Overall yield = 80 %;

DOI:10.1002/bkcs.11673

upstream raw materials:

N-(propyl)chloroacetamide

2,4-dichlorophenol

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