4-methoxy-11-[4-methoxy-phenyl]-11,12-dihydro-6H-dibenz[b,f][1,5]oxazocine

Base Information

Chemical Name:4-methoxy-11-[4-methoxy-phenyl]-11,12-dihydro-6H-dibenz[b,f][1,5]oxazocine
CAS No.:1297529-95-3
Molecular Formula:C₂₂H₂₁NO₃
Molecular Weight:347.414
Hs Code.:

Synonyms:4-methoxy-11-[4-methoxy-phenyl]-11,12-dihydro-6H-dibenz[b,f][1,5]oxazocine

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Chemical Property of 4-methoxy-11-[4-methoxy-phenyl]-11,12-dihydro-6H-dibenz[b,f][1,5]oxazocine

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Technology Process of 4-methoxy-11-[4-methoxy-phenyl]-11,12-dihydro-6H-dibenz[b,f][1,5]oxazocine

There total 5 articles about 4-methoxy-11-[4-methoxy-phenyl]-11,12-dihydro-6H-dibenz[b,f][1,5]oxazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1297529-87-3
[2-(2-bromo-benzyloxy)-3-methoxy-benzyl]-(4-methoxyphenyl)-amine

: 1297529-95-3
4-methoxy-11-[4-methoxy-phenyl]-11,12-dihydro-6H-dibenz[b,f][1,5]oxazocine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; for 15h; Reflux; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.02.024

Reference yield:

: 728885-46-9
2-(2-bromobenzyloxy)-3-methoxybenzaldehyde

: 1297529-95-3
4-methoxy-11-[4-methoxy-phenyl]-11,12-dihydro-6H-dibenz[b,f][1,5]oxazocine

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 12 h / 25 °C

2: sodium tetrahydroborate / ethanol / 2 h / 0 °C

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 15 h / Reflux; Inert atmosphere

With sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In ethanol;
DOI:10.1016/j.ejmech.2011.02.024

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 1297529-95-3
4-methoxy-11-[4-methoxy-phenyl]-11,12-dihydro-6H-dibenz[b,f][1,5]oxazocine

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 3 h / Reflux

2: ethanol / 12 h / 25 °C

3: sodium tetrahydroborate / ethanol / 2 h / 0 °C

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 15 h / Reflux; Inert atmosphere

With sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In ethanol; acetone;
DOI:10.1016/j.ejmech.2011.02.024