methyl 2-acetoxy-6-((R,E)-4-(tert-butyldimethylsilyloxy)hept-1-enyl)-3,4-dimethoxybenzoate

Base Information

Chemical Name:methyl 2-acetoxy-6-((R,E)-4-(tert-butyldimethylsilyloxy)hept-1-enyl)-3,4-dimethoxybenzoate
CAS No.:1360789-69-0
Molecular Formula:C₂₅H₄₀O₇Si
Molecular Weight:480.674
Hs Code.:

Synonyms:methyl 2-acetoxy-6-((R,E)-4-(tert-butyldimethylsilyloxy)hept-1-enyl)-3,4-dimethoxybenzoate

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Chemical Property of methyl 2-acetoxy-6-((R,E)-4-(tert-butyldimethylsilyloxy)hept-1-enyl)-3,4-dimethoxybenzoate

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Technology Process of methyl 2-acetoxy-6-((R,E)-4-(tert-butyldimethylsilyloxy)hept-1-enyl)-3,4-dimethoxybenzoate

There total 4 articles about methyl 2-acetoxy-6-((R,E)-4-(tert-butyldimethylsilyloxy)hept-1-enyl)-3,4-dimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1360789-68-9
C₂₃H₃₈O₆Si

: 108-24-7
acetic anhydride

: 1360789-69-0
methyl 2-acetoxy-6-((R,E)-4-(tert-butyldimethylsilyloxy)hept-1-enyl)-3,4-dimethoxybenzoate

Guidance literature:: With pyridine;
DOI:10.1021/ol300185u

Reference yield:

: 1360789-61-2
(R)-4-(tert-butyldimethylsilyloxy)-(E)-hept-1-enylboronic acid

: 1360789-69-0
methyl 2-acetoxy-6-((R,E)-4-(tert-butyldimethylsilyloxy)hept-1-enyl)-3,4-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; potassium carbonate; triphenylphosphine / 1,2-dimethoxyethane; water / 2.5 h / 80 °C / Inert atmosphere

2: pyridine

With pyridine; palladium diacetate; potassium carbonate; triphenylphosphine; In 1,2-dimethoxyethane; water;
DOI:10.1021/ol300185u

Reference yield:

: 1752-02-9
methyl 6-iodo-2,3,4-trimethoxybenzoate

: 1360789-69-0
methyl 2-acetoxy-6-((R,E)-4-(tert-butyldimethylsilyloxy)hept-1-enyl)-3,4-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: boron tribromide / dichloromethane

2: palladium diacetate; potassium carbonate; triphenylphosphine / 1,2-dimethoxyethane; water / 2.5 h / 80 °C / Inert atmosphere

3: pyridine

With pyridine; palladium diacetate; boron tribromide; potassium carbonate; triphenylphosphine; In 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1021/ol300185u