N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]-4-nitrobenzamide

Base Information

Chemical Name:N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]-4-nitrobenzamide
CAS No.:1267507-99-2
Molecular Formula:C₁₆H₇Cl₂F₇N₂O₃
Molecular Weight:479.138
Hs Code.:

Synonyms:N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]-4-nitrobenzamide

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Chemical Property of N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]-4-nitrobenzamide

Chemical Property:

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Technology Process of N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]-4-nitrobenzamide

There total 1 articles about N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]-4-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.4%

: 273735-64-1
2,6-dichloro-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]aniline

: 122-04-3
4-nitro-benzoyl chloride

: 1267507-99-2
N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]-4-nitrobenzamide

Guidance literature:: With pyridine; for 3h; Reflux;

Reference yield: 96.0%

: 1267507-99-2
N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]-4-nitrobenzamide

: 1267508-04-2
4-amino-N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]benzamide

Guidance literature:: N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]-4-nitrobenzamide; With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In methanol; at 20 ℃; Cooling with ice;

With ammonia; In methanol; water;

Reference yield:

: 1267507-99-2
N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]-4-nitrobenzamide

: 1267507-92-5
3-chloro-4-cyano-N-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol / 20 °C / Cooling with ice

2: N-chloro-succinimide / toluene / 6 h / 80 °C

3: diiodomethane; tert.-butylnitrite / acetonitrile / 20 - 60 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 7 h / 80 °C / Inert atmosphere

With sodium tetrahydroborate; N-chloro-succinimide; tert.-butylnitrite; nickel(II) chloride hexahydrate; diiodomethane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; N,N-dimethyl-formamide; toluene; acetonitrile;