(3RS,9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-3-methyl-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinolinium iodide

Base Information

Chemical Name:(3RS,9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-3-methyl-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinolinium iodide
CAS No.:133964-06-4
Molecular Formula:C₂₂H₂₅N₂O₃*I
Molecular Weight:492.357
Hs Code.:

Synonyms:(3RS,9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-3-methyl-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinolinium iodide

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Chemical Property of (3RS,9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-3-methyl-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinolinium iodide

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Technology Process of (3RS,9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-3-methyl-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinolinium iodide

There total 3 articles about (3RS,9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-3-methyl-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinolinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 133964-05-3
(9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinoline

: 74-88-4
methyl iodide

: 133964-06-4
(3RS,9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-3-methyl-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinolinium iodide

Guidance literature:: for 8h; Heating;
DOI:10.1021/jo00015a025

Reference yield:

: 123420-50-8
8,9-dimethoxy-2,3,5,6-tetrahydro-1H-pyrrolo[2,1-a]isoquinolinium; bromide

: 133964-06-4
(3RS,9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-3-methyl-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinolinium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Et₃N / CHCl₃ / 1) ice bath, 0.5 h, 2) 25 deg C, 1 h

2: 94 percent / 8 h / Heating

With triethylamine; In chloroform;
DOI:10.1021/jo00015a025

Reference yield:

: 698-16-8
benzohydroximoyl chloride

: 133964-06-4
(3RS,9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-3-methyl-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinolinium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Et₃N / CHCl₃ / 1) ice bath, 0.5 h, 2) 25 deg C, 1 h

2: 94 percent / 8 h / Heating

With triethylamine; In chloroform;
DOI:10.1021/jo00015a025