2-ethoxycarbonyl-4-(2-furyl)-6-(4-methoxyphenyl)-5-methyl-2H-1,3-oxazine

Base Information

Chemical Name:2-ethoxycarbonyl-4-(2-furyl)-6-(4-methoxyphenyl)-5-methyl-2H-1,3-oxazine
CAS No.:175727-87-4
Molecular Formula:C₁₉H₁₉NO₅
Molecular Weight:341.364
Hs Code.:

Synonyms:2-ethoxycarbonyl-4-(2-furyl)-6-(4-methoxyphenyl)-5-methyl-2H-1,3-oxazine

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Chemical Property of 2-ethoxycarbonyl-4-(2-furyl)-6-(4-methoxyphenyl)-5-methyl-2H-1,3-oxazine

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Technology Process of 2-ethoxycarbonyl-4-(2-furyl)-6-(4-methoxyphenyl)-5-methyl-2H-1,3-oxazine

There total 1 articles about 2-ethoxycarbonyl-4-(2-furyl)-6-(4-methoxyphenyl)-5-methyl-2H-1,3-oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 924-44-7
glyoxylic acid ethyl ester

: 175727-87-4
2-ethoxycarbonyl-4-(2-furyl)-6-(4-methoxyphenyl)-5-methyl-2H-1,3-oxazine

Guidance literature:: In tetrahydrofuran; Ambient temperature;
DOI:10.1016/0040-4020(95)01097-1

Reference yield: 79.0%

: 175727-87-4
2-ethoxycarbonyl-4-(2-furyl)-6-(4-methoxyphenyl)-5-methyl-2H-1,3-oxazine

: (1S,2R,3R/1R,2S,3S)-3-ethoxycarbonylmethylamino-3-(2-furyl)-1-(4-methoxyphenyl)-1-propanol

Guidance literature:: With sodium cyanoborohydride; acetic acid; In tetrahydrofuran; Ambient temperature;
DOI:10.1016/0040-4020(95)01097-1

Reference yield:

: 175727-87-4
2-ethoxycarbonyl-4-(2-furyl)-6-(4-methoxyphenyl)-5-methyl-2H-1,3-oxazine

: (2R,3R,4R/2S,3S,4S)-1-ethoxycarbonylmethyl-2-furyl-4-(4-methoxyphenyl)-3-methylazetidine

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / NaBH₃CN, AcOH / tetrahydrofuran / Ambient temperature

2: NEt₃, DMAP / CH₂Cl₂ / 2 h / 0 °C

3: aq. NaHCO₃

With dmap; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0040-4020(95)01097-1