Ethyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

Base Information

Chemical Name:Ethyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside
CAS No.:162316-86-1
Molecular Formula:C₄₅H₄₈O₇SSi
Molecular Weight:761.023
Hs Code.:

Synonyms:Ethyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

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Chemical Property of Ethyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

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Technology Process of Ethyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

There total 3 articles about Ethyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 162316-82-7
Ethyl 2,3-di-O-benzoyl-4-O-benzyl-1-thio-α-D-glucopyranoside

: 162316-86-1
Ethyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 70 ℃; for 1h;

Reference yield:

: 98-88-4
benzoyl chloride

: 162316-86-1
Ethyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / pyridine / 5 h / Ambient temperature

2: 1.) BH₃*Me₃N, molecular sieves 4 Angstroem, 2.) AlCl₃ / 1.) PhMe, r.t., 1 h, 2.) r.t., 2 h

3: 92 percent / imidazole / dimethylformamide / 1 h / 70 °C

With pyridine; 1H-imidazole; aluminium trichloride; trimethylamine-borane; 4 A molecular sieve; In N,N-dimethyl-formamide;

Reference yield:

: 162427-46-5
Ethyl 2,3-di-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-glucopyranoside

: 162316-86-1
Ethyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BH₃*Me₃N, molecular sieves 4 Angstroem, 2.) AlCl₃ / 1.) PhMe, r.t., 1 h, 2.) r.t., 2 h

2: 92 percent / imidazole / dimethylformamide / 1 h / 70 °C

With 1H-imidazole; aluminium trichloride; trimethylamine-borane; 4 A molecular sieve; In N,N-dimethyl-formamide;