2,2'-(2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(4-(4-chlorophenyl)decahydroquinoline)

Base Information

Chemical Name:2,2'-(2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(4-(4-chlorophenyl)decahydroquinoline)
CAS No.:1447968-13-9
Molecular Formula:C₃₈H₄₉Cl₂N₃
Molecular Weight:618.733
Hs Code.:

Synonyms:2,2'-(2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(4-(4-chlorophenyl)decahydroquinoline)

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Chemical Property of 2,2'-(2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(4-(4-chlorophenyl)decahydroquinoline)

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Technology Process of 2,2'-(2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(4-(4-chlorophenyl)decahydroquinoline)

There total 4 articles about 2,2'-(2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(4-(4-chlorophenyl)decahydroquinoline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1447968-11-7
2,2'-((2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(1-(4-chlorophenyl)-3-oxopropane-3,1-diyl))dicyclohexanone

: 1447968-13-9
2,2'-(2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(4-(4-chlorophenyl)decahydroquinoline)

Guidance literature:: With ammonium acetate; acetic acid; Reflux;
DOI:10.1016/j.saa.2012.12.069

Reference yield:

: 1447967-99-8
(2E,2'E)-1,1'-(2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(3-(4-chlorophenyl)prop-2-en-1-one)

: 1447968-13-9
2,2'-(2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(4-(4-chlorophenyl)decahydroquinoline)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium ethanolate / ethanol / 6 h / Reflux

2: acetic acid; ammonium acetate / Reflux

With ammonium acetate; sodium ethanolate; acetic acid; In ethanol; 1: |Michael Addition;
DOI:10.1016/j.saa.2012.12.069

Reference yield:

: 1081-09-0
3,5-diacetyl-1,4-dihydro-2,4,6-trimethylpyridine

: 1447968-13-9
2,2'-(2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(4-(4-chlorophenyl)decahydroquinoline)

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / 20 °C

2: sodium ethanolate / ethanol / 6 h / Reflux

3: acetic acid; ammonium acetate / Reflux

With ammonium acetate; sodium ethanolate; acetic acid; potassium hydroxide; In ethanol; 2: |Michael Addition;
DOI:10.1016/j.saa.2012.12.069