2,2'-((2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(1-(4-chlorophenyl)-3-oxopropane-3,1-diyl))dicyclohexanone

Base Information

Chemical Name:2,2'-((2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(1-(4-chlorophenyl)-3-oxopropane-3,1-diyl))dicyclohexanone
CAS No.:1447968-11-7
Molecular Formula:C₃₈H₄₃Cl₂NO₄
Molecular Weight:648.67
Hs Code.:

Synonyms:2,2'-((2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(1-(4-chlorophenyl)-3-oxopropane-3,1-diyl))dicyclohexanone

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Chemical Property of 2,2'-((2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(1-(4-chlorophenyl)-3-oxopropane-3,1-diyl))dicyclohexanone

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Technology Process of 2,2'-((2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(1-(4-chlorophenyl)-3-oxopropane-3,1-diyl))dicyclohexanone

There total 3 articles about 2,2'-((2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(1-(4-chlorophenyl)-3-oxopropane-3,1-diyl))dicyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1447967-99-8
(2E,2'E)-1,1'-(2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(3-(4-chlorophenyl)prop-2-en-1-one)

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1447968-11-7
2,2'-((2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(1-(4-chlorophenyl)-3-oxopropane-3,1-diyl))dicyclohexanone

Guidance literature:: With sodium ethanolate; In ethanol; for 6h; Reflux;
DOI:10.1016/j.saa.2012.12.069

Reference yield:

: 1081-09-0
3,5-diacetyl-1,4-dihydro-2,4,6-trimethylpyridine

: 1447968-11-7
2,2'-((2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(1-(4-chlorophenyl)-3-oxopropane-3,1-diyl))dicyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / 20 °C

2: sodium ethanolate / ethanol / 6 h / Reflux

With sodium ethanolate; potassium hydroxide; In ethanol; 2: |Michael Addition;
DOI:10.1016/j.saa.2012.12.069

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1447968-11-7
2,2'-((2,4,6-trimethyl-1,4-dihydropyridine-3,5-diyl)bis(1-(4-chlorophenyl)-3-oxopropane-3,1-diyl))dicyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / 20 °C

2: sodium ethanolate / ethanol / 6 h / Reflux

With sodium ethanolate; potassium hydroxide; In ethanol; 2: |Michael Addition;
DOI:10.1016/j.saa.2012.12.069