tert-butyl [2-(2-chlorophenyl)ethyl]{3-[(2-oxoethyl)thio]propyl}carbamate

Base Information

Chemical Name:tert-butyl [2-(2-chlorophenyl)ethyl]{3-[(2-oxoethyl)thio]propyl}carbamate
CAS No.:928628-28-8
Molecular Formula:C₁₈H₂₆ClNO₃S
Molecular Weight:371.928
Hs Code.:

Synonyms:tert-butyl [2-(2-chlorophenyl)ethyl]{3-[(2-oxoethyl)thio]propyl}carbamate

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Chemical Property of tert-butyl [2-(2-chlorophenyl)ethyl]{3-[(2-oxoethyl)thio]propyl}carbamate

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Technology Process of tert-butyl [2-(2-chlorophenyl)ethyl]{3-[(2-oxoethyl)thio]propyl}carbamate

There total 12 articles about tert-butyl [2-(2-chlorophenyl)ethyl]{3-[(2-oxoethyl)thio]propyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 928628-27-7
tert-butyl [2-(2-chlorophenyl)ethyl]{3-[(2-hydroxyethyl)thio]propyl}carbamate

: 928628-28-8
tert-butyl [2-(2-chlorophenyl)ethyl]{3-[(2-oxoethyl)thio]propyl}carbamate

Guidance literature:: With sulfur trioxide pyridine complex; triethylamine; In dimethyl sulfoxide; at 25 ℃; for 0.666667h; Product distribution / selectivity;

Reference yield:

: 13078-80-3
2-(2-chlorophenyl)ethanamine

: 928628-28-8
tert-butyl [2-(2-chlorophenyl)ethyl]{3-[(2-oxoethyl)thio]propyl}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine

2: sodium hydride

3: 2,2'-azobis(isobutyronitrile)

4: sulfur trioxide pyridine complex

With 2,2'-azobis(isobutyronitrile); sulfur trioxide pyridine complex; sodium hydride; triethylamine;
DOI:10.1016/j.bmcl.2011.05.097

Reference yield:

: 928628-25-5
tert-butyl allyl[2-(2-chlorophenyl)ethyl]carbamate

: 928628-28-8
tert-butyl [2-(2-chlorophenyl)ethyl]{3-[(2-oxoethyl)thio]propyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2'-azobis(isobutyronitrile)

2: sulfur trioxide pyridine complex

With 2,2'-azobis(isobutyronitrile); sulfur trioxide pyridine complex;
DOI:10.1016/j.bmcl.2011.05.097