2-Acetyl-5-hydroxy-6-(2-carboxy-6-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:2-Acetyl-5-hydroxy-6-(2-carboxy-6-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene
CAS No.:97006-25-2
Molecular Formula:C₂₁H₂₀O₆
Molecular Weight:368.386
Hs Code.:

Synonyms:2-Acetyl-5-hydroxy-6-(2-carboxy-6-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene

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Chemical Property of 2-Acetyl-5-hydroxy-6-(2-carboxy-6-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene

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Technology Process of 2-Acetyl-5-hydroxy-6-(2-carboxy-6-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene

There total 7 articles about 2-Acetyl-5-hydroxy-6-(2-carboxy-6-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 97006-24-1
2-Acetyl-5-hydroxy-6-(2-carbomethoxy-6-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene

: 97006-25-2
2-Acetyl-5-hydroxy-6-(2-carboxy-6-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With sodium hydroxide; In ethanol; for 4h; Heating;

Reference yield:

: 83344-22-3
2-Acetyl-8-bromo-5-hydroxy-1,2,3,4-tetrahydronaphthalene-4-one

: 97006-25-2
2-Acetyl-5-hydroxy-6-(2-carboxy-6-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 4 steps

1: 45 percent / H₂ / PtO₂ / ethanol / 6 h / 760 Torr

2: 90 percent / (CF₃CO)2O / CH₂Cl₂ / 4 h / Ambient temperature

3: 60 percent / BF₃*Et₂O / 0.08 h / 130 °C

4: 94 percent / 8percent aq. NaOH / ethanol / 4 h / Heating

With sodium hydroxide; boron trifluoride diethyl etherate; hydrogen; trifluoroacetic anhydride; platinum(IV) oxide; In ethanol; dichloromethane;

Reference yield:

: 83344-21-2
3-Acetyl-4-(2-bromo-5-hydroxyphenyl)butyric acid

: 97006-25-2
2-Acetyl-5-hydroxy-6-(2-carboxy-6-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / conc. H₂SO₄ / 1) 0 deg C 2) 4h, room temperature

2: 45 percent / H₂ / PtO₂ / ethanol / 6 h / 760 Torr

3: 90 percent / (CF₃CO)2O / CH₂Cl₂ / 4 h / Ambient temperature

4: 60 percent / BF₃*Et₂O / 0.08 h / 130 °C

5: 94 percent / 8percent aq. NaOH / ethanol / 4 h / Heating

With sodium hydroxide; sulfuric acid; boron trifluoride diethyl etherate; hydrogen; trifluoroacetic anhydride; platinum(IV) oxide; In ethanol; dichloromethane;