CuC₁₂H₆N₂(C₆H₄)2(CH₂)10O₆C₁₂H₆N₂(C₆H₄)2(CH₂)10O₄C₆H₄C(C₆H₄C(CH₃)3)3SCOCH₃⁽¹⁺⁾*BF₄^(1-)

Base Information

• Chemical Name: CuC₁₂H₆N₂(C₆H₄)2(CH₂)10O₆C₁₂H₆N₂(C₆H₄)2(CH₂)10O₄C₆H₄C(C₆H₄C(CH₃)3)3SCOCH₃⁽¹⁺⁾*BF₄^(1-)
• CAS No.: 611198-96-0
• Molecular Formula: BF₄*C₁₀₇H₁₁₄CuN₄O₁₁S
• Molecular Weight: 1814.52

Synonyms:CuC₁₂H₆N₂(C₆H₄)2(CH₂)10O₆C₁₂H₆N₂(C₆H₄)2(CH₂)10O₄C₆H₄C(C₆H₄C(CH₃)3)3SCOCH₃⁽¹⁺⁾*BF₄^(1-)

Chemical Property of CuC₁₂H₆N₂(C₆H₄)2(CH₂)10O₆C₁₂H₆N₂(C₆H₄)2(CH₂)10O₄C₆H₄C(C₆H₄C(CH₃)3)3SCOCH₃⁽¹⁺⁾*BF₄^(1-)

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Technology Process of CuC₁₂H₆N₂(C₆H₄)2(CH₂)10O₆C₁₂H₆N₂(C₆H₄)2(CH₂)10O₄C₆H₄C(C₆H₄C(CH₃)3)3SCOCH₃⁽¹⁺⁾*BF₄^(1-)

There total 1 articles about CuC₁₂H₆N₂(C₆H₄)2(CH₂)10O₆C₁₂H₆N₂(C₆H₄)2(CH₂)10O₄C₆H₄C(C₆H₄C(CH₃)3)3SCOCH₃⁽¹⁺⁾*BF₄^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrakis(acetonitrile)copper(I)tetrafluoroborate + C12H6N2(C6H4)2(CH2)10O4SCOCH3C6H4C(C6H4C(CH3)3)3 (611198-91-5) + ((C2H4O)2C6H4)NC5H2C2H2C5H2N(C6H4(C2H4O)2)OC2H4O (90030-13-0) → CuC12H6N2(C6H4)2(CH2)10O6C12H6N2(C6H4)2(CH2)10O4C6H4C(C6H4C(CH3)3)3SCOCH3(1+)*BF4(1-) (611198-96-0)

Guidance literature:

In dichloromethane; acetonitrile; Cu-complex in MeCN was added under Ar at room temp. to stirred soln. of ligand in CH2Cl2, 15 min at room temp., second ligand in CH2Cl2 was added, stirred for 2 h under Ar at room temp.; solvents were removed in vac.;

DOI:10.1021/ic0347034

Reference yield: 53.0%

CuC12H6N2(C6H4)2(CH2)10O6C12H6N2(C6H4)2(CH2)10O4C6H4C(C6H4C(CH3)3)3SCOCH3(1+)*BF4(1-) (611198-96-0) → 2Cu(1+)*2C12H6N2(C6H4)2(CH2)10O6*(C12H6N2(C6H4)2(CH2)10O4C6H4C(C6H4C(CH3)3)3S)2*2BF4(1-)

Guidance literature:

With dmap; tetrafluoroboric acid; In tetrahydrofuran; methanol; MeOH and DMAP were added to soln. fo Cu-complex in THF, HBF4 was added, heated to 60°C for 5 d under Ar; solvent was removed, taken up into CH2Cl2/H2O, dried over Na2SO4, solvent was removed, chromd. on Al2O3 with CH2Cl2/MeOH;

DOI:10.1021/ic0347034

upstream raw materials:

C₁₂H₆N₂(C₆H₄)2(CH₂)10O₄SCOCH₃C₆H₄C(C₆H₄C(CH₃)3)3

((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

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