(p-aminophenylthiolato-S)(N-ethyl-N,N-bis(ethylene-2-thiolato-S)amino-N)oxorhenium(V)

Base Information

• Chemical Name: (p-aminophenylthiolato-S)(N-ethyl-N,N-bis(ethylene-2-thiolato-S)amino-N)oxorhenium(V)
• CAS No.: 221100-14-7
• Molecular Formula: C₁₂H₁₉N₂OReS₃
• Molecular Weight: 489.701

Synonyms:(p-aminophenylthiolato-S)(N-ethyl-N,N-bis(ethylene-2-thiolato-S)amino-N)oxorhenium(V)

Chemical Property of (p-aminophenylthiolato-S)(N-ethyl-N,N-bis(ethylene-2-thiolato-S)amino-N)oxorhenium(V)

Chemical Property:

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Technology Process of (p-aminophenylthiolato-S)(N-ethyl-N,N-bis(ethylene-2-thiolato-S)amino-N)oxorhenium(V)

There total 1 articles about (p-aminophenylthiolato-S)(N-ethyl-N,N-bis(ethylene-2-thiolato-S)amino-N)oxorhenium(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

[ReOCl3(PPh3)2] + N,N-bis(2-mercaptoethyl)ethylamine (4410-96-2) + 4-aminotiophenol (1193-02-8) → (p-aminophenylthiolato-S)(N-ethyl-N,N-bis(ethylene-2-thiolato-S)amino-N)oxorhenium(V) (221100-14-7)

Guidance literature:

With AcONa; In methanol; dropwise addn. of ligand precursors to soln. of Re-complex contg. AcONa (stirring), refluxing to dissoln.; water addn., extn. into CH2Cl2, drying (MgSO4), concn., crystn. on MeOHaddn. and slow evapn.; elem. anal.;

DOI:10.1016/s0020-1693(98)00330-2

Reference yield: 80.0%

(p-aminophenylthiolato-S)(N-ethyl-N,N-bis(ethylene-2-thiolato-S)amino-N)oxorhenium(V) (221100-14-7) + benzoyl chloride (98-88-4) → ReO(C2H5N(CH2CH2S)2)(SC6H4NHCOC6H5) (259260-93-0)

Guidance literature:

With iPr₂NEt; In chloroform; crystn. on slow evapn. (CHCl3 / EtOH); elem. anal.;

DOI:10.1016/S0277-5387(99)00286-7

upstream raw materials:

N,N-bis(2-mercaptoethyl)ethylamine

4-aminotiophenol

Downstream raw materials:

ReO(C₂H₅N(CH₂CH₂S)2)(SC₆H₄NHCOC₆H₅)

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