(2S,6S)-2,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,5,6-tetrahydropyridine-3-carboxylic acid ethyl ester

Base Information

Chemical Name:(2S,6S)-2,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,5,6-tetrahydropyridine-3-carboxylic acid ethyl ester
CAS No.:528853-89-6
Molecular Formula:C₂₇H₂₇NO₄S
Molecular Weight:461.582
Hs Code.:

Synonyms:(2S,6S)-2,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,5,6-tetrahydropyridine-3-carboxylic acid ethyl ester

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Chemical Property of (2S,6S)-2,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,5,6-tetrahydropyridine-3-carboxylic acid ethyl ester

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Technology Process of (2S,6S)-2,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,5,6-tetrahydropyridine-3-carboxylic acid ethyl ester

There total 2 articles about (2S,6S)-2,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,5,6-tetrahydropyridine-3-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 51608-60-7
N-(benzylidene)-p-methylbenzenesulfonamide

: 433733-19-8
2-benzyl-buta-2,3-dienoic acid ethyl ester

: (2R,6R)-2,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,5,6-tetrahydropyridine-3-carboxylic acid ethyl ester

: 528853-89-6
(2S,6S)-2,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,5,6-tetrahydropyridine-3-carboxylic acid ethyl ester

Guidance literature:: With C₂₇H₂₆F₆NOP; In dichloromethane; at 20 ℃; for 16h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/chem.201100850

Reference yield:

: 51608-60-7
phenyl N-tosyl imine

: 433733-19-8
2-benzyl-buta-2,3-dienoic acid ethyl ester

: (2R,6R)-2,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,5,6-tetrahydropyridine-3-carboxylic acid ethyl ester

: 528853-89-6
(2S,6S)-2,6-diphenyl-1-(toluene-4-sulfonyl)-1,2,5,6-tetrahydropyridine-3-carboxylic acid ethyl ester

Guidance literature:: With (R)-BINAP tert-butyl-phosphine derivative; In dichloromethane; at 20 ℃; for 16h; Title compound not separated from byproducts;
DOI:10.1021/ja053277d