⁽⁰⁸¹⁾C₀₇₅₀₆

Base Information

Chemical Name:⁽⁰⁸¹⁾C₀₇₅₀₆
CAS No.:1147015-37-9
Molecular Formula:C₁₇H₁₅ClN₆
Molecular Weight:338.799
Hs Code.:

Synonyms:⁽⁰⁸¹⁾C₀₇₅₀₆

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Chemical Property of ⁽⁰⁸¹⁾C₀₇₅₀₆

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Technology Process of ⁽⁰⁸¹⁾C₀₇₅₀₆

There total 4 articles about ⁽⁰⁸¹⁾C₀₇₅₀₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1147015-36-8
2-[4-(2-methyl-imidazol-1-ylmethyl)-phenylamino]-7H-pyrrolo[2,3-d]pyrimidin-4-ol

⁽⁰⁸¹⁾C₀₇₅₀₆: 1147015-37-9
⁽⁰⁸¹⁾C₀₇₅₀₆

Guidance literature:: 2-[4-(2-methyl-imidazol-1-ylmethyl)-phenylamino]-7H-pyrrolo[2,3-d]pyrimidin-4-ol; With trichlorophosphate; at 120 ℃; for 0.5h;

at 0 ℃; pH=9 - 10; Alkaline aqueous solution;

Reference yield:

: 1143571-99-6
(E)-tert-butyl (tert-butoxycarbonylamino)(4-((2-methyl-1H-imidazol-1-yl)methyl)phenylamino)methylenecarbamate

⁽⁰⁸¹⁾C₀₇₅₀₆: 1147015-37-9
⁽⁰⁸¹⁾C₀₇₅₀₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 1.5 h

2.1: sodium methylate / methanol / 0.5 h / 150 °C / Microwave irradiation

3.1: trichlorophosphate / 0.5 h / 120 °C

3.2: 0 °C / pH 9 - 10

With sodium methylate; trifluoroacetic acid; trichlorophosphate; In methanol; dichloromethane;

Reference yield:

: 1142947-77-0
1-(4-((2-methyl-1H-imidazol-1-yl)methyl)phenyl)guanidine

⁽⁰⁸¹⁾C₀₇₅₀₆: 1147015-37-9
⁽⁰⁸¹⁾C₀₇₅₀₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 0.5 h / 150 °C / Microwave irradiation

2.1: trichlorophosphate / 0.5 h / 120 °C

2.2: 0 °C / pH 9 - 10

With sodium methylate; trichlorophosphate; In methanol;