Technology Process of 4-octyl-1-(phenylselanylmethyl)-1,2,3-triazole
There total 3 articles about 4-octyl-1-(phenylselanylmethyl)-1,2,3-triazole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(II) acetate monohydrate; sodium L-ascorbate;
In
tetrahydrofuran; water;
at 20 ℃;
for 8h;
DOI:10.1016/j.tet.2012.07.019
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate / ethanol / Reflux
2: sodium azide; 18-crown-6 ether / acetonitrile / 48 h / 20 °C / Inert atmosphere
3: sodium L-ascorbate; copper(II) acetate monohydrate / tetrahydrofuran; water / 8 h / 20 °C
With
sodium tetrahydroborate; sodium azide; 18-crown-6 ether; copper(II) acetate monohydrate; sodium L-ascorbate;
In
tetrahydrofuran; ethanol; water; acetonitrile;
3: |Huisgen Cycloaddition;
DOI:10.1016/j.tet.2012.07.019
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide; 18-crown-6 ether / acetonitrile / 48 h / 20 °C / Inert atmosphere
2: sodium L-ascorbate; copper(II) acetate monohydrate / tetrahydrofuran; water / 8 h / 20 °C
With
sodium azide; 18-crown-6 ether; copper(II) acetate monohydrate; sodium L-ascorbate;
In
tetrahydrofuran; water; acetonitrile;
2: |Huisgen Cycloaddition;
DOI:10.1016/j.tet.2012.07.019
