13-cyclohexyl-6-(1H-tetrazol-5-yl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester

Base Information

Chemical Name:13-cyclohexyl-6-(1H-tetrazol-5-yl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester
CAS No.:945626-73-3
Molecular Formula:C₂₆H₂₅N₅O₂
Molecular Weight:439.517
Hs Code.:

Synonyms:13-cyclohexyl-6-(1H-tetrazol-5-yl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester

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Chemical Property of 13-cyclohexyl-6-(1H-tetrazol-5-yl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester

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Technology Process of 13-cyclohexyl-6-(1H-tetrazol-5-yl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester

There total 1 articles about 13-cyclohexyl-6-(1H-tetrazol-5-yl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 877287-32-6
6-cyano-13-cyclohexyl-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester

: 945626-73-3
13-cyclohexyl-6-(1H-tetrazol-5-yl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester

Guidance literature:: 6-cyano-13-cyclohexyl-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester; With azido tributyltin (IV); In toluene; at 150 ℃; for 0.5h; Microwave irradiation;

With hydrogenchloride; water; In toluene;

Reference yield: 49.0%

: 945626-73-3
13-cyclohexyl-6-(1H-tetrazol-5-yl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester

: 107-07-3
2-chloro-ethanol

: 13-cyclohexyl-6-[2-(2-hydroxyethyl)-2H-tetrazol-5-yl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid

Guidance literature:: 13-cyclohexyl-6-(1H-tetrazol-5-yl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester; 2-chloro-ethanol; With caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 18h;

With water; caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 8h;

With hydrogenchloride; In water; N,N-dimethyl-formamide;

Reference yield: 48.0%

: 1192-30-9
tetrahydrofurfuryl bromide

: 945626-73-3
13-cyclohexyl-6-(1H-tetrazol-5-yl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester

: 13-cyclohexyl-6-[1-[(tetrahydro-2-furanyl)methyl]-1H-tetrazol-5-yl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid

: 13-cyclohexyl-6-[2-[(tetrahydro-2-furanyl)methyl]-2H-tetrazol-5-yl]-5H-indolo[2,1-a][2]benzazepine-10-carboxylic acid

: 13-cyclohexyl-6-[2-[(tetrahydro-2-furanyl)methyl]-2H-tetrazol-5-yl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid

Guidance literature:: tetrahydrofurfuryl bromide; 13-cyclohexyl-6-(1H-tetrazol-5-yl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid methyl ester; With caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 18h;

With water; caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 8h;

With hydrogenchloride; In water; N,N-dimethyl-formamide;