4-((4S)-methoxy-(2S)-pyrrolidinylmethoxy)benzoic acid ethyl ester-1-carboxylic acid benzyl ester

Base Information

Chemical Name:4-((4S)-methoxy-(2S)-pyrrolidinylmethoxy)benzoic acid ethyl ester-1-carboxylic acid benzyl ester
CAS No.:792916-41-7
Molecular Formula:C₂₃H₂₇NO₆
Molecular Weight:413.47
Hs Code.:

Synonyms:4-((4S)-methoxy-(2S)-pyrrolidinylmethoxy)benzoic acid ethyl ester-1-carboxylic acid benzyl ester

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Chemical Property of 4-((4S)-methoxy-(2S)-pyrrolidinylmethoxy)benzoic acid ethyl ester-1-carboxylic acid benzyl ester

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Technology Process of 4-((4S)-methoxy-(2S)-pyrrolidinylmethoxy)benzoic acid ethyl ester-1-carboxylic acid benzyl ester

There total 2 articles about 4-((4S)-methoxy-(2S)-pyrrolidinylmethoxy)benzoic acid ethyl ester-1-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.9%

: 792916-40-6
ethyl 4-(N-benzyloxycarbonyl-(4S)-hydroxy-(2S)-pyrrolidinylmethoxy)benzoate

: 74-88-4
methyl iodide

: 792916-41-7
4-((4S)-methoxy-(2S)-pyrrolidinylmethoxy)benzoic acid ethyl ester-1-carboxylic acid benzyl ester

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3.5h;

Reference yield:

: 120-47-8
Ethyl 4-hydroxybenzoate

: 858971-58-1
(4S)-methoxy-(2S)-(p-toluenesulfonyloxymethyl)pyrrolidine-1-carboxylic acid benzyl ester

: 792916-41-7
4-((4S)-methoxy-(2S)-pyrrolidinylmethoxy)benzoic acid ethyl ester-1-carboxylic acid benzyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 - 80 ℃;

Reference yield: 60.2%

: 792916-41-7
4-((4S)-methoxy-(2S)-pyrrolidinylmethoxy)benzoic acid ethyl ester-1-carboxylic acid benzyl ester

: 144-62-7,97993-78-7
oxalic acid

: 858971-59-2
4-((4S)-methoxy-(2S)-pyrrolidinylmethoxy)benzoic acid ethyl ester·oxalic acid salt

Guidance literature:: 4-((4S)-methoxy-(2S)-pyrrolidinylmethoxy)benzoic acid ethyl ester-1-carboxylic acid benzyl ester; With hydrogen; palladium over charcoal; In ethanol; for 5h;

oxalic acid; In ethanol; at 0 ℃; for 3h;