(-)-menthyl mesityl-2-hydroxy-5-trifluoromethyl phenyl phosphinate

Base Information

Chemical Name:(-)-menthyl mesityl-2-hydroxy-5-trifluoromethyl phenyl phosphinate
CAS No.:1464049-27-1
Molecular Formula:C₂₆H₃₄F₃O₃P
Molecular Weight:482.523
Hs Code.:

Synonyms:(-)-menthyl mesityl-2-hydroxy-5-trifluoromethyl phenyl phosphinate

Suppliers and Price of (-)-menthyl mesityl-2-hydroxy-5-trifluoromethyl phenyl phosphinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of (-)-menthyl mesityl-2-hydroxy-5-trifluoromethyl phenyl phosphinate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of (-)-menthyl mesityl-2-hydroxy-5-trifluoromethyl phenyl phosphinate

There total 2 articles about (-)-menthyl mesityl-2-hydroxy-5-trifluoromethyl phenyl phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: (-)-menthyl O-4-(trifluoromethyl)phenyl 2,4,6-trimethylphenylphosphonate

: 1464049-27-1
(-)-menthyl mesityl-2-hydroxy-5-trifluoromethyl phenyl phosphinate

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; at -78 ℃; for 1h; stereospecific reaction; Inert atmosphere;
DOI:10.1002/adsc.201300913

Reference yield:

: 1061745-76-3
(-)-menthyl (Rp)-mesitylphosphinate

: 1464049-27-1
(-)-menthyl mesityl-2-hydroxy-5-trifluoromethyl phenyl phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrachloromethane / 20 °C / Inert atmosphere

2: diisopropylamine; n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

With n-butyllithium; triethylamine; diisopropylamine; In tetrahydrofuran; tetrachloromethane;
DOI:10.1002/adsc.201300913