[(E)-N,N'-bis(4-chloro-6-methoxy-1,3,5-triazin-2-yl)-4,4'-azobenzenedicarboxamide]-[α-cyclodextrin]-[2]-[rotaxane]

Base Information

• Chemical Name: [(E)-N,N'-bis(4-chloro-6-methoxy-1,3,5-triazin-2-yl)-4,4'-azobenzenedicarboxamide]-[α-cyclodextrin]-[2]-[rotaxane]
• CAS No.: 1034911-61-9
• Molecular Formula: C₂₀H₁₆Cl₂N₁₀O₂*C₃₆H₆₀O₃₀
• Molecular Weight: 1472.17

Synonyms:[(E)-N,N'-bis(4-chloro-6-methoxy-1,3,5-triazin-2-yl)-4,4'-azobenzenedicarboxamide]-[α-cyclodextrin]-[2]-[rotaxane]

Chemical Property of [(E)-N,N'-bis(4-chloro-6-methoxy-1,3,5-triazin-2-yl)-4,4'-azobenzenedicarboxamide]-[α-cyclodextrin]-[2]-[rotaxane]

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Technology Process of [(E)-N,N'-bis(4-chloro-6-methoxy-1,3,5-triazin-2-yl)-4,4'-azobenzenedicarboxamide]-[α-cyclodextrin]-[2]-[rotaxane]

There total 1 articles about [(E)-N,N'-bis(4-chloro-6-methoxy-1,3,5-triazin-2-yl)-4,4'-azobenzenedicarboxamide]-[α-cyclodextrin]-[2]-[rotaxane] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

2,4-Dichloro-6-methoxy-1,3,5-triazine (3638-04-8) + 4,4'-Diaminoazobenzene (538-41-0) + alpha cyclodextrin (10016-20-3) → [(E)-N,N'-bis(4-chloro-6-methoxy-1,3,5-triazin-2-yl)-4,4'-azobenzenedicarboxamide]-[α-cyclodextrin]-[2]-[rotaxane] (1034911-61-9)

Guidance literature:

4,4'-Diaminoazobenzene; alpha cyclodextrin; With triethylamine; In water; at 20 ℃; for 2h; pH=10;

2,4-Dichloro-6-methoxy-1,3,5-triazine; In water; at 20 ℃; for 12h;

DOI:10.1039/b802229a

Reference yield: 76.0%

[(E)-N,N'-bis(4-chloro-6-methoxy-1,3,5-triazin-2-yl)-4,4'-azobenzenedicarboxamide]-[α-cyclodextrin]-[2]-[rotaxane] (1034911-61-9) + Trimethylenediamine (109-76-2,54018-94-9) → [(E)-N,N'-bis(4-(3-aminopropylamino)-6-methoxy-1,3,5-triazin-2-yl)-4,4'-azobenzenedicarboxamide]-[α-cyclodextrin]-[2]-[rotaxane] (1034911-68-6)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 10h;

DOI:10.1039/b802229a

upstream raw materials:

2,4-Dichloro-6-methoxy-1,3,5-triazine

4,4'-Diaminoazobenzene

alpha cyclodextrin

Downstream raw materials:

[(E)-N,N'-bis(4-(3-aminopropylamino)-6-methoxy-1,3,5-triazin-2-yl)-4,4'-azobenzenedicarboxamide]-[α-cyclodextrin]-[2]-[rotaxane]

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