(N(2,6-i-Pr₂C₆H₃)C(Me)CHC(Me)N(2,6-i-Pr₂C₆H₃))GeOH

Base Information

Chemical Name:(N(2,6-i-Pr₂C₆H₃)C(Me)CHC(Me)N(2,6-i-Pr₂C₆H₃))GeOH
CAS No.:692776-46-8
Molecular Formula:C₂₉H₄₂GeN₂O
Molecular Weight:507.255
Hs Code.:

(N(2,6-i-Pr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>)C(Me)CHC(Me)N(2,6-i-Pr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>))GeOH

Synonyms:(N(2,6-i-Pr₂C₆H₃)C(Me)CHC(Me)N(2,6-i-Pr₂C₆H₃))GeOH

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Chemical Property of (N(2,6-i-Pr₂C₆H₃)C(Me)CHC(Me)N(2,6-i-Pr₂C₆H₃))GeOH

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Technology Process of (N(2,6-i-Pr₂C₆H₃)C(Me)CHC(Me)N(2,6-i-Pr₂C₆H₃))GeOH

There total 4 articles about (N(2,6-i-Pr₂C₆H₃)C(Me)CHC(Me)N(2,6-i-Pr₂C₆H₃))GeOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 908373-69-3
[((2,6-(i-Pr)2C₆H₃)NC(=CH₂)CH=C(Me)N(2,6-(i-Pr)2C₆H₃))Ge]

: 7732-18-5
water

: 692776-46-8
(N(2,6-i-Pr₂C₆H₃)C(Me)CHC(Me)N(2,6-i-Pr₂C₆H₃))GeOH

Guidance literature:: In water; toluene; (N2); Schlenk technique; H2O (1 equiv.) was added with stirring to soln.of Ge compd. (1 equiv.) in toluene at room temp.; stirred for 15 min; evapd. (vac.); extd. (hexane); concd.; stored at -30°C for 1 d;
DOI:10.1021/om900149k

Reference yield: 84.0%

: 334719-93-6
[C₃H(CH₃)2(N(2,6-diisopropylphenyl))2 chlorogermylene]

: 7732-18-5
water

: 692776-46-8
(N(2,6-i-Pr₂C₆H₃)C(Me)CHC(Me)N(2,6-i-Pr₂C₆H₃))GeOH

Guidance literature:: With 1,3-dimesitylimidazol-2-ylidene; In toluene; byproducts: 1,3-dimesitylimidazolium chloride; under inert atm.; Ge-comp. and imidazolydene dissolved in toluene at room temp., H2O slowly added, stirred for ca. 15 min; filtered in vacuo, evapd., rinsed with hexane, dried in vacuo; elem. anal.;
DOI:10.1002/anie.200353205

Reference yield:

: 334719-93-6
[C₃H(CH₃)2(N(2,6-diisopropylphenyl))2 chlorogermylene]

: 692776-46-8
(N(2,6-i-Pr₂C₆H₃)C(Me)CHC(Me)N(2,6-i-Pr₂C₆H₃))GeOH

Guidance literature:: Multi-step reaction with 3 steps

1: toluene

2: 1,3-di-tert-butylimidazol-2-ylidene / toluene

3: water; toluene

With 1,3-di-tert-butylimidazol-2-ylidene; In water; toluene;
DOI:10.1021/om900149k