methyl α-((p-benzyloxy)phenyl)-α-(3-methyl-3-(phenylthio)-2-oxo-1-azetidinyl)acetate

Base Information

Chemical Name:methyl α-((p-benzyloxy)phenyl)-α-(3-methyl-3-(phenylthio)-2-oxo-1-azetidinyl)acetate
CAS No.:87568-51-2
Molecular Formula:C₂₆H₂₅NO₄S
Molecular Weight:447.555
Hs Code.:

Synonyms:methyl α-((p-benzyloxy)phenyl)-α-(3-methyl-3-(phenylthio)-2-oxo-1-azetidinyl)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl α-((p-benzyloxy)phenyl)-α-(3-methyl-3-(phenylthio)-2-oxo-1-azetidinyl)acetate

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Technology Process of methyl α-((p-benzyloxy)phenyl)-α-(3-methyl-3-(phenylthio)-2-oxo-1-azetidinyl)acetate

There total 1 articles about methyl α-((p-benzyloxy)phenyl)-α-(3-methyl-3-(phenylthio)-2-oxo-1-azetidinyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87568-48-7
methyl D-α-methylacrylamido-α-((p-benzyloxy)phenyl)acetate

: 931-59-9
benzenesulfenyl chloride

: 87568-51-2
methyl α-((p-benzyloxy)phenyl)-α-(3-methyl-3-(phenylthio)-2-oxo-1-azetidinyl)acetate

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) CH₂Cl₂, 0 deg C, 3 h, 2.) C₆H₆, DMF, 0 deg C, 1 h;
DOI:10.1021/ja00363a023

Reference yield: 82.0%

: 87568-51-2
methyl α-((p-benzyloxy)phenyl)-α-(3-methyl-3-(phenylthio)-2-oxo-1-azetidinyl)acetate

: 87568-52-3
(R)-(3-Benzenesulfinyl-3-methyl-2-oxo-azetidin-1-yl)-(4-benzyloxy-phenyl)-acetic acid methyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃; for 0.25h;
DOI:10.1021/ja00363a023

Reference yield:

: 87568-51-2
methyl α-((p-benzyloxy)phenyl)-α-(3-methyl-3-(phenylthio)-2-oxo-1-azetidinyl)acetate

: 87568-53-4
methyl α-((p-benzyloxy)phenyl)-1-(3-methylene-2-oxoazetidinyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / MCPBA / CH₂Cl₂ / 0.25 h / -78 °C

2: 50 percent / toluene / 20 h / Heating

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1021/ja00363a023