C₃₇H₄₂N₈O₆S₂

Base Information

Chemical Name:C₃₇H₄₂N₈O₆S₂
CAS No.:1588427-99-9
Molecular Formula:C₃₇H₄₂N₈O₆S₂
Molecular Weight:758.922
Hs Code.:

C<sub>37</sub>H<sub>42</sub>N<sub>8</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₃₇H₄₂N₈O₆S₂

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Chemical Property of C₃₇H₄₂N₈O₆S₂

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Technology Process of C₃₇H₄₂N₈O₆S₂

There total 10 articles about C₃₇H₄₂N₈O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1588428-16-3
C₃₇H₄₄N₈O₇S₂

: 1588427-99-9
C₃₇H₄₂N₈O₆S₂

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In dichloromethane; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.02.106

Reference yield:

: 1146435-74-6
C₁₃H₂₂N₂O₄S

: 1588427-99-9
C₃₇H₄₂N₈O₆S₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridine; trifluoroacetic anhydride / 1,2-dimethoxyethane / 3.5 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: trifluoroacetic acid; methoxybenzene / dichloromethane / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: trifluoroacetic acid; methoxybenzene / dichloromethane / Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dichloromethane / 1 h / 20 °C / Inert atmosphere

6.1: lithium hydroxide; dihydrogen peroxide / ethanol / 0 °C / Inert atmosphere

6.2: pH 1 / Inert atmosphere

7.1: trifluoroacetic acid; methoxybenzene / dichloromethane / Inert atmosphere

8.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / dichloromethane / Inert atmosphere

With pyridine; dihydrogen peroxide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; trifluoroacetic anhydride; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; lithium hydroxide; In 1,2-dimethoxyethane; ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2014.02.106

Reference yield:

: 96929-06-5
ethyl 2-<(S)-1-(N-t-butoxycarbonyl)aminoethyl>thiazole-4-carboxylate

: 1588427-99-9
C₃₇H₄₂N₈O₆S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: trifluoroacetic acid; methoxybenzene / dichloromethane / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: trifluoroacetic acid; methoxybenzene / dichloromethane / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dichloromethane / 1 h / 20 °C / Inert atmosphere

5.1: lithium hydroxide; dihydrogen peroxide / ethanol / 0 °C / Inert atmosphere

5.2: pH 1 / Inert atmosphere

6.1: trifluoroacetic acid; methoxybenzene / dichloromethane / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / dichloromethane / Inert atmosphere

With dihydrogen peroxide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; lithium hydroxide; In ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2014.02.106