[4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde dimethyl acetal

Base Information

• Chemical Name: [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde dimethyl acetal
• CAS No.: 73182-14-6
• Molecular Formula: C₂₁H₂₄N₂O₄S
• Molecular Weight: 400.499

Synonyms:[4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde dimethyl acetal

Chemical Property of [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde dimethyl acetal

Chemical Property:

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Technology Process of [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde dimethyl acetal

There total 2 articles about [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloroacetaldehyde dimethyl acetal (97-97-2) + 4,5-bis(4-methoxyphenyl)-2-mercapto-1H-imidazole (39908-69-5) → [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde dimethyl acetal (73182-14-6)

Guidance literature:

In N-methyl-acetamide; water;

Reference yield:

→ [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde dimethyl acetal (73182-14-6)

Guidance literature:

/BRN= 620430/, NaH, ClCH2CH(OCH3)2;

Reference yield:

[4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde dimethyl acetal (73182-14-6) → 2-(2,2-dimethoxy-ethanesulfinyl)-4,5-bis-(4-methoxy-phenyl)-1H-imidazole

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

upstream raw materials:

chloroacetaldehyde dimethyl acetal

4,5-bis(4-methoxyphenyl)-2-mercapto-1H-imidazole

Downstream raw materials:

2-(2,2-dimethoxy-ethanesulfonyl)-4,5-bis-(4-methoxy-phenyl)-1H-imidazole

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