ethyl 2,6-dideoxy-3,4-bis-O-(p-methoxybenzoyl)-1-thio-α-D-ribo-hexopyranoside

Base Information

• Chemical Name: ethyl 2,6-dideoxy-3,4-bis-O-(p-methoxybenzoyl)-1-thio-α-D-ribo-hexopyranoside
• CAS No.: 91732-82-0
• Molecular Formula: C₂₄H₂₈O₇S
• Molecular Weight: 460.548
• Mol file: 91732-82-0.mol

Synonyms:ethyl 2,6-dideoxy-3,4-bis-O-(p-methoxybenzoyl)-1-thio-α-D-ribo-hexopyranoside

Chemical Property of ethyl 2,6-dideoxy-3,4-bis-O-(p-methoxybenzoyl)-1-thio-α-D-ribo-hexopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 2,6-dideoxy-3,4-bis-O-(p-methoxybenzoyl)-1-thio-α-D-ribo-hexopyranoside

There total 3 articles about ethyl 2,6-dideoxy-3,4-bis-O-(p-methoxybenzoyl)-1-thio-α-D-ribo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-benzoyl chloride (100-07-2) → ethyl 2,6-dideoxy-3,4-bis-O-(p-methoxybenzoyl)-1-thio-α-D-ribo-hexopyranoside (91732-82-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 94 percent / pyridine / 6 h / Ambient temperature

2: 4.7 g / H₂O / acetic acid / 2 h / Heating

3: TsOH / CH₂Cl₂ / 20 h / Ambient temperature

With water; toluene-4-sulfonic acid; In pyridine; dichloromethane; acetic acid;

DOI:10.1002/hlca.19850680203

Reference yield:

methyl 2,6-dideoxy-3,4-bis-O-(p-methoxybenzoyl)-α-D-ribo-hexopyranoside (98292-31-0) → ethyl 2,6-dideoxy-3,4-bis-O-(p-methoxybenzoyl)-1-thio-α-D-ribo-hexopyranoside (91732-82-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 4.7 g / H₂O / acetic acid / 2 h / Heating

2: TsOH / CH₂Cl₂ / 20 h / Ambient temperature

With water; toluene-4-sulfonic acid; In dichloromethane; acetic acid;

DOI:10.1002/hlca.19850680203

Reference yield:

methyl 2,6-dideoxy-α-D-ribo-hexopyranoside (4092-45-9,13322-79-7,17676-16-3,17676-19-6,19131-10-3,19131-11-4,33985-35-2,40878-56-6,53293-94-0,56733-47-2,62346-15-0,71305-70-9,72204-04-7,77210-24-3,78853-88-0,92007-64-2,133814-52-5,139756-72-2) → ethyl 2,6-dideoxy-3,4-bis-O-(p-methoxybenzoyl)-1-thio-α-D-ribo-hexopyranoside (91732-82-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 94 percent / pyridine / 6 h / Ambient temperature

2: 4.7 g / H₂O / acetic acid / 2 h / Heating

3: TsOH / CH₂Cl₂ / 20 h / Ambient temperature

With water; toluene-4-sulfonic acid; In pyridine; dichloromethane; acetic acid;

DOI:10.1002/hlca.19850680203

upstream raw materials:

4-methoxy-benzoyl chloride

methyl 2,6-dideoxy-3,4-bis-O-(p-methoxybenzoyl)-α-D-ribo-hexopyranoside

methyl 2,6-dideoxy-α-D-ribo-hexopyranoside