2-[1-(4-Dimethylamino-phenyl)-meth-(E)-ylidene]-4-oxo-4-phenyl-butyric acid hydrazide

Base Information

Chemical Name:2-[1-(4-Dimethylamino-phenyl)-meth-(E)-ylidene]-4-oxo-4-phenyl-butyric acid hydrazide
CAS No.:654075-44-2
Molecular Formula:C₁₉H₂₁N₃O₂
Molecular Weight:323.395
Hs Code.:

Synonyms:2-[1-(4-Dimethylamino-phenyl)-meth-(E)-ylidene]-4-oxo-4-phenyl-butyric acid hydrazide

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Chemical Property of 2-[1-(4-Dimethylamino-phenyl)-meth-(E)-ylidene]-4-oxo-4-phenyl-butyric acid hydrazide

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Technology Process of 2-[1-(4-Dimethylamino-phenyl)-meth-(E)-ylidene]-4-oxo-4-phenyl-butyric acid hydrazide

There total 1 articles about 2-[1-(4-Dimethylamino-phenyl)-meth-(E)-ylidene]-4-oxo-4-phenyl-butyric acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: (E)-3-(4-(dimethylamino)benzylidene)-5-phenylfuran-2(3H)-one

: 654075-44-2
2-[1-(4-Dimethylamino-phenyl)-meth-(E)-ylidene]-4-oxo-4-phenyl-butyric acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; at 25 ℃; for 12h;
DOI:10.1002/hc.10197

Reference yield: 31.0%

: 98-88-4
benzoyl chloride

: 654075-44-2
2-[1-(4-Dimethylamino-phenyl)-meth-(E)-ylidene]-4-oxo-4-phenyl-butyric acid hydrazide

: 654075-50-0
Benzoic acid N'-{2-[1-(4-dimethylamino-phenyl)-meth-(E)-ylidene]-4-oxo-4-phenyl-butyryl}-hydrazide

Guidance literature:: In benzene; at 75 ℃; for 6h;
DOI:10.1002/hc.10197

Reference yield:

: 654075-44-2
2-[1-(4-Dimethylamino-phenyl)-meth-(E)-ylidene]-4-oxo-4-phenyl-butyric acid hydrazide

: (E)-4-(4-Dimethylamino-phenyl)-1-phenyl-3-(5-phenyl-[1,3,4]oxadiazol-2-yl)-but-3-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 31 percent / benzene / 6 h / 75 °C

2: 26.6 percent / phosphorus oxychloride / 1 h / Heating

With trichlorophosphate; In benzene;
DOI:10.1002/hc.10197