3-O-benzoyl-2-deoxy-4,5-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

Base Information

• Chemical Name: 3-O-benzoyl-2-deoxy-4,5-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile
• CAS No.: 1053238-14-4
• Molecular Formula: C₁₈H₂₁NO₇
• Molecular Weight: 363.367

Synonyms:3-O-benzoyl-2-deoxy-4,5-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

Chemical Property of 3-O-benzoyl-2-deoxy-4,5-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

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Technology Process of 3-O-benzoyl-2-deoxy-4,5-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

There total 1 articles about 3-O-benzoyl-2-deoxy-4,5-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3-O-benzoyl-2-deoxy-4,5:6,8-di-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile (724766-07-8) → 3-O-benzoyl-2-deoxy-4,5-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile (1053238-14-4)

Guidance literature:

With acetic acid; at 50 ℃; for 4h;

DOI:10.1016/j.tet.2008.06.021

Reference yield: 85.0%

3-O-benzoyl-2-deoxy-4,5-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile (1053238-14-4) → 3-O-benzoyl-2-deoxy-8-azido-4,5-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile (1053238-16-6)

Guidance literature:

With 1H-imidazole; iodine; triphenylphosphine; In toluene; at 100 ℃; for 2h;

DOI:10.1016/j.tet.2008.06.021

Reference yield: 81.0%

3-O-benzoyl-2-deoxy-4,5-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile (1053238-14-4) + p-toluenesulfonyl chloride (98-59-9) → 3-O-benzoyl-2-deoxy-4,5-O-isopropylidene-8-O-p-toluenesulfonyl-α-L-gulo-oct-4-ulo-4,7-furanosononitrile (1053238-15-5)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 1.5h;

DOI:10.1016/j.tet.2008.06.021

upstream raw materials:

3-O-benzoyl-2-deoxy-4,5:6,8-di-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

Downstream raw materials:

3-O-benzoyl-2-deoxy-8-azido-4,5-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

3-O-benzoyl-2-deoxy-4,5-O-isopropylidene-8-O-p-toluenesulfonyl-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

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