3-O-benzoyl-2-deoxy-4,5:6,8-di-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

Base Information

Chemical Name:3-O-benzoyl-2-deoxy-4,5:6,8-di-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile
CAS No.:724766-07-8
Molecular Formula:C₂₁H₂₅NO₇
Molecular Weight:403.432
Hs Code.:

Synonyms:3-O-benzoyl-2-deoxy-4,5:6,8-di-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

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Chemical Property of 3-O-benzoyl-2-deoxy-4,5:6,8-di-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

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Technology Process of 3-O-benzoyl-2-deoxy-4,5:6,8-di-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

There total 2 articles about 3-O-benzoyl-2-deoxy-4,5:6,8-di-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 98-88-4
benzoyl chloride

: 724766-05-6
2-deoxy-4,5:6,8-di-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

: 724766-07-8
3-O-benzoyl-2-deoxy-4,5:6,8-di-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

Guidance literature:: With triethylamine; In dichloromethane; for 6h;
DOI:10.1055/s-2004-822328

Reference yield:

: 55385-72-3
(3aS,3bR,7aS,8aR)-2,2,5,5-tetramethyltetrahydro-8aH-[1,3]dioxolo[4′,5′:4,5]furo[3,2-d][1,3]dioxine-8a-carbaldehyde

: 724766-07-8
3-O-benzoyl-2-deoxy-4,5:6,8-di-O-isopropylidene-α-L-gulo-oct-4-ulo-4,7-furanosononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: Zn-Cu; I₂ / dioxane / 2 h / 80 °C

2: 72 percent / Et₃N / CH₂Cl₂ / 6 h

With iodine; copper; triethylamine; zinc; In 1,4-dioxane; dichloromethane; 1: Reformatsky reaction;
DOI:10.1055/s-2004-822328