1,2-bis{4-[1-(6-phenoxyhexyl)-1,2,3-triazol-4-yl]phenyl}-1,2-diphenylethene

Base Information

Chemical Name:1,2-bis{4-[1-(6-phenoxyhexyl)-1,2,3-triazol-4-yl]phenyl}-1,2-diphenylethene
CAS No.:1380324-43-5
Molecular Formula:C₅₄H₅₄N₆O₂
Molecular Weight:819.062
Hs Code.:

Synonyms:1,2-bis{4-[1-(6-phenoxyhexyl)-1,2,3-triazol-4-yl]phenyl}-1,2-diphenylethene

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Chemical Property of 1,2-bis{4-[1-(6-phenoxyhexyl)-1,2,3-triazol-4-yl]phenyl}-1,2-diphenylethene

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Technology Process of 1,2-bis{4-[1-(6-phenoxyhexyl)-1,2,3-triazol-4-yl]phenyl}-1,2-diphenylethene

There total 7 articles about 1,2-bis{4-[1-(6-phenoxyhexyl)-1,2,3-triazol-4-yl]phenyl}-1,2-diphenylethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.8%

: 1032300-86-9
((6-azidohexyl)oxy)benzene

: 1240785-42-5
1,2-bis(4-ethynylphenyl)-1,2-diphenyl-ethene

: 1380324-43-5
1,2-bis{4-[1-(6-phenoxyhexyl)-1,2,3-triazol-4-yl]phenyl}-1,2-diphenylethene

Guidance literature:: With bromotris(triphenylphosphine)copper(I); In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;
DOI:10.1039/c0jm04100a

Reference yield:

: 629-03-8
1 ,6-dibromohexane

: 1380324-43-5
1,2-bis{4-[1-(6-phenoxyhexyl)-1,2,3-triazol-4-yl]phenyl}-1,2-diphenylethene

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 26 h / Reflux

2: sodium azide / dimethyl sulfoxide / 20 °C

3: bromotris(triphenylphosphine)copper(I) / N,N-dimethyl-formamide / 60 °C / Inert atmosphere

With sodium azide; bromotris(triphenylphosphine)copper(I); potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c0jm04100a

Reference yield:

: 1263774-65-7
1,2-bis{4-[2-(trimethylsilyl)ethynyl]phenyl}-1,2-diphenylethene

: 1380324-43-5
1,2-bis{4-[1-(6-phenoxyhexyl)-1,2,3-triazol-4-yl]phenyl}-1,2-diphenylethene

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; potassium hydroxide / tetrahydrofuran / 20 °C

2: bromotris(triphenylphosphine)copper(I) / N,N-dimethyl-formamide / 60 °C / Inert atmosphere

With methanol; bromotris(triphenylphosphine)copper(I); potassium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c0jm04100a