C₁₅H₁₃ClN₂O₄

Base Information

Chemical Name:C₁₅H₁₃ClN₂O₄
CAS No.:1426319-63-2
Molecular Formula:C₁₅H₁₃ClN₂O₄
Molecular Weight:320.732
Hs Code.:

C<sub>15</sub>H<sub>13</sub>ClN<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₅H₁₃ClN₂O₄

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Chemical Property of C₁₅H₁₃ClN₂O₄

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Technology Process of C₁₅H₁₃ClN₂O₄

There total 7 articles about C₁₅H₁₃ClN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1426320-74-2
C₁₆H₁₅ClN₂O₄

: 1426319-63-2
C₁₅H₁₃ClN₂O₄

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 4h;

Reference yield:

: 89694-47-3
(4-chloro-3-methoxyphenyl)boronic acid

: 1426319-63-2
C₁₅H₁₃ClN₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane / 3 h / 90 °C / Inert atmosphere

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / 16 h / 50 °C / 3750.38 Torr / Inert atmosphere

3: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

4: sulfuric acid / 4 h / Reflux

5: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

6: sodium hydroxide / tetrahydrofuran / 4 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; di-isopropyl azodicarboxylate; sulfuric acid; boron tribromide; potassium carbonate; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane;

Reference yield:

: 1426320-72-0
C₁₁H₇ClN₂O₃

: 1426319-63-2
C₁₅H₁₃ClN₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 4 h / Reflux

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: sodium hydroxide / tetrahydrofuran / 4 h / 20 °C

With di-isopropyl azodicarboxylate; sulfuric acid; triphenylphosphine; sodium hydroxide; In tetrahydrofuran;