tert-butyl 4'-<<<<1-<(fluorenylmethyloxycarbonyl)amino>cyclopentyl>carbonyl>amino>methyl>biphenyl-2-carboxylate

Base Information

Chemical Name:tert-butyl 4'-<<<<1-<(fluorenylmethyloxycarbonyl)amino>cyclopentyl>carbonyl>amino>methyl>biphenyl-2-carboxylate
CAS No.:151257-02-2
Molecular Formula:C₃₉H₄₀N₂O₅
Molecular Weight:616.757
Hs Code.:

Synonyms:tert-butyl 4'-<<<<1-<(fluorenylmethyloxycarbonyl)amino>cyclopentyl>carbonyl>amino>methyl>biphenyl-2-carboxylate

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Chemical Property of tert-butyl 4'-<<<<1-<(fluorenylmethyloxycarbonyl)amino>cyclopentyl>carbonyl>amino>methyl>biphenyl-2-carboxylate

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Technology Process of tert-butyl 4'-<<<<1-<(fluorenylmethyloxycarbonyl)amino>cyclopentyl>carbonyl>amino>methyl>biphenyl-2-carboxylate

There total 3 articles about tert-butyl 4'-<<<<1-<(fluorenylmethyloxycarbonyl)amino>cyclopentyl>carbonyl>amino>methyl>biphenyl-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 117322-30-2
1-<(fluorenylmethyloxycarbonyl)amino>cyclopentane-1-carboxylic acid

: 133690-73-0
4'-(Aminomethyl)[1,1'-biphenyl]-2-carboxylic acid,1,1-dimethylethyl ester

: 151257-02-2
tert-butyl 4'-<<<<1-<(fluorenylmethyloxycarbonyl)amino>cyclopentyl>carbonyl>amino>methyl>biphenyl-2-carboxylate

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; diethylamine; In N,N-dimethyl-formamide; for 1h;
DOI:10.1021/jm00074a018

Reference yield:

: 139476-12-3
4'-(Azidomethyl)[1,1'-biphenyl]-2-carboxylic acid,1,1-dimethylethyl ester

: 151257-02-2
tert-butyl 4'-<<<<1-<(fluorenylmethyloxycarbonyl)amino>cyclopentyl>carbonyl>amino>methyl>biphenyl-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Ph₃P, 2.) H₂O / 1.) THF, 25 deg C, 3 h, 2.) THF, 18 h

2: 97 percent / <(benzotriazol-1-yl)oxy>tris(dimethylamino)phosphonium hexafluorophosphate (BOP), Et₂NH / dimethylformamide / 1 h

With water; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; diethylamine; triphenylphosphine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00074a018